(+/-)-2--3-methyl-1-butanol

Base Information

Chemical Name:(+/-)-2--3-methyl-1-butanol
CAS No.:127180-91-0
Molecular Formula:C₁₂H₁₇NO₃
Molecular Weight:223.272
Hs Code.:

(+/-)-2-<N-(benzoyloxy)amino>-3-methyl-1-butanol

Synonyms:(+/-)-2--3-methyl-1-butanol

Suppliers and Price of (+/-)-2--3-methyl-1-butanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-2--3-methyl-1-butanol

Chemical Property:

Purity/Quality:

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Technology Process of (+/-)-2--3-methyl-1-butanol

There total 3 articles about (+/-)-2--3-methyl-1-butanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 16369-05-4,473-75-6
valinol

: 94-36-0
dibenzoyl peroxide

: 127180-91-0
(+/-)-2--3-methyl-1-butanol

Guidance literature:: With disodium hydrogenphosphate; In tetrahydrofuran; at 25 ℃; for 3h;
DOI:10.1021/jo00298a018

Reference yield:

: 13893-45-3
valine ethyl ester

: 127180-91-0
(+/-)-2--3-methyl-1-butanol

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / LiAlH₄

2: 56 percent / Na₂HPO₄ / tetrahydrofuran / 3 h / 25 °C

With disodium hydrogenphosphate; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jo00298a018

Reference yield:

: 516-06-3,25609-85-2,7004-03-7,921-10-8
D,L-valine

: 127180-91-0
(+/-)-2--3-methyl-1-butanol

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent

2: 82 percent / LiAlH₄

3: 56 percent / Na₂HPO₄ / tetrahydrofuran / 3 h / 25 °C

With disodium hydrogenphosphate; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jo00298a018