methyl 1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolinate

Base Information

Chemical Name:methyl 1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolinate
CAS No.:1482285-98-2
Molecular Formula:C₁₉H₂₃BrN₂O₅
Molecular Weight:439.306
Hs Code.:

Synonyms:methyl 1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolinate

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Chemical Property of methyl 1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolinate

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Technology Process of methyl 1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolinate

There total 1 articles about methyl 1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 586-76-5
4-Bromobenzoic acid

: 323207-12-1
methyl (S)-N-(1-aza-6-oxaspiro[2.5]oct-1-en-2-yl)prolinate

: 1482285-98-2
methyl 1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolinate

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 45h;
DOI:10.1002/hlca.201300062

Reference yield: 98.0%

: 1482285-98-2
methyl 1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolinate

: 1482285-99-3
1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-proline

Guidance literature:: With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; at 20 ℃; for 23h;
DOI:10.1002/hlca.201300062

Reference yield:

: 1482285-98-2
methyl 1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolinate

: 1482286-00-9
methyl 1-[(4-{[1-({4-[(4-bromobenzoyl)amino]-3,4,5,6-tetrahydro-2H-pyran-4-yl}carbonyl)-L-prolyl]amino}-3,4,5,6-tetrahydro-2H-pyran-4-yl)carbonyl]-L-prolinate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 23 h / 20 °C

2: tetrahydrofuran / 47 h / 0 - 20 °C

With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol;
DOI:10.1002/hlca.201300062