Benzaldehyde, 4-chloro-, 5-(4-chlorophenyl)methylene-4,5-dihydro-4-oxo-2-thiazolylhydrazone

Base Information

Chemical Name:Benzaldehyde, 4-chloro-, 5-(4-chlorophenyl)methylene-4,5-dihydro-4-oxo-2-thiazolylhydrazone
CAS No.:904-60-9
Molecular Formula:C₁₇H₁₁Cl₂N₃OS
Molecular Weight:376.266
Hs Code.:
Mol file:904-60-9.mol

Synonyms:Benzaldehyde,4-chloro-, [5-[(4-chlorophenyl)methylene]-4,5-dihydro-4-oxo-2-thiazolyl]hydrazone(9CI); Benzaldehyde, p-chloro-, 2-azine with5-(p-chlorobenzylidene)-2,4-thiazolidinedione (7CI,8CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzaldehyde, 4-chloro-, 5-(4-chlorophenyl)methylene-4,5-dihydro-4-oxo-2-thiazolylhydrazone

Chemical Property:

PSA：79.12000
LogP:4.91620

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 4-chloro-, 5-(4-chlorophenyl)methylene-4,5-dihydro-4-oxo-2-thiazolylhydrazone

There total 6 articles about Benzaldehyde, 4-chloro-, 5-(4-chlorophenyl)methylene-4,5-dihydro-4-oxo-2-thiazolylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 32003-36-4
2-hydrazino-1,3-thiazol-4(5H)-one

: 104-88-1
4-chlorobenzaldehyde

: 904-60-9
5-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-2-{N'-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazino}-thiazol-4-one

Guidance literature:: With triethylamine; In ethanol; for 3h; Heating;

Reference yield:

: 5349-28-0
thiocyanato-acetic acid ethyl ester

: 3510-48-3,41097-37-4
4-chlorobenzaldehyde azine

: 904-60-9
4-chloro-benzaldehyde [5-(4-chloro-benzylidene)-4-oxo-thiazolidin-2-ylidene]-hydrazone

Guidance literature:: With hydrazine hydrate; In acetic acid; for 8h; Heating;
DOI:10.1246/bcsj.45.952

Reference yield:

: 5706-80-9
4-chlorobenzaldehyde thiosemicarbazone

: 904-60-9
4-chloro-benzaldehyde [5-(4-chloro-benzylidene)-4-oxo-thiazolidin-2-ylidene]-hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: NaOAc / ethanol / Heating

2: NaOAc / acetic acid / Heating

With sodium acetate; In ethanol; acetic acid;