cyclohexylcarbonyl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide

Base Information

Chemical Name:cyclohexylcarbonyl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide
CAS No.:473440-42-5
Molecular Formula:C₁₂H₂₁O₃PS₂
Molecular Weight:308.403
Hs Code.:

Synonyms:cyclohexylcarbonyl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide

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Chemical Property of cyclohexylcarbonyl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide

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Technology Process of cyclohexylcarbonyl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide

There total 2 articles about cyclohexylcarbonyl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.4%

: 697-45-0
5,5-dimethyl-2-thiolo-2-thiono-1,3,2-dioxaphosphorinane

: 2719-27-9
cyclohexanylcarbonyl chloride

: 473440-42-5
cyclohexylcarbonyl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide

Guidance literature:: With triethylamine; In benzene; for 0.25h; cooling;
DOI:10.1081/SCC-120018942

Reference yield:

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 473440-42-5
cyclohexylcarbonyl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 79.7 percent / P₂S₅ / benzene / 50 °C

2: 93 percent / Et₃N / benzene / 0.25 h / ice-cooling

With tetraphosphorus decasulfide; triethylamine; In benzene;
DOI:10.1039/b201233b