N-METHYL-3-PYRROLIDINOL

Base Information Edit

Chemical Name:N-METHYL-3-PYRROLIDINOL
CAS No.:99445-21-3
Molecular Formula:C₅H₁₁NO
Molecular Weight:101.148
Hs Code.:
Mol file:99445-21-3.mol

Synonyms:1-Methyl-3-hydroxypyrrolidine;1-Methyl-3-pyrrolidinol; 3-Hydroxy-1-methylpyrrolidine;3-Hydroxy-N-methylpyrrolidine; N-Methyl-3-hydroxypyrrolidine;N-Methyl-3-pyrrolidinol; NSC 89279

Suppliers and Price of N-METHYL-3-PYRROLIDINOL

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 17 raw suppliers

Chemical Property of N-METHYL-3-PYRROLIDINOL Edit

Chemical Property:

Vapor Pressure:0.132mmHg at 25°C
Boiling Point:192.2°C at 760 mmHg
Flash Point:70.6°C
PSA：23.47000
Density:1.045±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:-0.37930

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s): R36/37/38:;
Hazard Codes: Xi:Irritant;
Statements: R36/37/38:;
Safety Statements: S26:; S36/37/39:;

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-METHYL-3-PYRROLIDINOL

There total 24 articles about N-METHYL-3-PYRROLIDINOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 19398-47-1,1360729-08-3
1,4-dibromo-2-butanol

: 74-89-5
methylamine

: 13220-33-2,99445-21-3
1-methyl-3-pyrrolidinol

: 1404453-61-7
1,4-bis(methylamino)butan-2-ol

Guidance literature:: In water; at 100 ℃; for 16h; Inert atmosphere;
DOI:10.1021/op3001788

Reference yield: 93.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 40499-83-0,83220-72-8,100243-39-8,2799-21-5
(3R)-pyrrolidinol

: 104641-60-3,99445-21-3
(R)-1-methyl-3-pyrrolidinol

Guidance literature:: formaldehyd; (3R)-pyrrolidinol; With platinum on carbon; hydrogen; In methanol; at 20 ℃; for 4h; under 3000.3 - 3750.38 Torr;

With diethylamine; In methanol; at 20 ℃; for 2.5h; under 3000.3 - 3750.38 Torr; Time; Reagent/catalyst;