2-bromo-2-boraadamantane

Base Information

Chemical Name:2-bromo-2-boraadamantane
CAS No.:76313-91-2
Molecular Formula:C₉H₁₄BBr
Molecular Weight:212.925
Hs Code.:

Synonyms:2-bromo-2-boraadamantane

Suppliers and Price of 2-bromo-2-boraadamantane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-bromo-2-boraadamantane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-bromo-2-boraadamantane

There total 2 articles about 2-bromo-2-boraadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 76313-88-7
2-isopropyl-2-boraadamantane

: 76313-91-2
2-bromo-2-boraadamantane

: 3α-bromo-7α-[(2-propyl)bromoboryl]bicyclo[3.3.1]nonane

: 4-ethoxy-5,5-dimethyl-4-borahomoadamantane

: 87367-47-3
3-noradamantylisopropylborinic acid

: 10035-10-6,12258-64-9
hydrogen bromide

Guidance literature:: With ethanol; water; bromine; In dichloromethane; water; byproducts: isopropylbromide; under Ar, to soln. of educt in CH2Cl2/H2O added with stirring over 1.5-3 h soln. of Br2 in CH2Cl2 at 0-2°C, stirred for 30 min, heated to room temp.; aq. layer removed, org. one washed with water, evapd., dissolved in ethanol; GLC anal. of products after oxidn. with H2O2/NaOH;
DOI:10.1016/0022-328X(83)85037-2

Reference yield: 73.0%

: 76313-88-7
2-isopropyl-2-boraadamantane

: 76313-91-2
2-bromo-2-boraadamantane

: 3α-bromo-7α-[(2-propyl)bromoboryl]bicyclo[3.3.1]nonane

: 4-ethoxy-5,5-dimethyl-4-borahomoadamantane

: 10035-10-6,12258-64-9
hydrogen bromide

: 75-26-3
isopropyl bromide

Guidance literature:: With ethanol; bromine; In dichloromethane; Irradiation (UV/VIS); under Ar, to soln. of educt in CH2Cl2 added soln. of Br2 in CH2Cl2 in portions during 1 h at -10°C under pressure of 170-200 mmHg with irrdn. with 200 W bulb, stirred for 30 min at -10°C, heated under vac. to 17°C; concd. in vac., cooled to -70°C, ethanol added, evapd. in vac. without heating; GLC anal. of products after oxidative hydrolysis;
DOI:10.1016/0022-328X(83)85037-2