αH-tetradecachloro-4-nitrotriphenylmethane

Base Information

• Chemical Name: αH-tetradecachloro-4-nitrotriphenylmethane
• CAS No.: 82891-75-6
• Molecular Formula: C₁₉HCl₁₄NO₂
• Molecular Weight: 771.564
• Mol file: 82891-75-6.mol

Synonyms:αH-tetradecachloro-4-nitrotriphenylmethane

Chemical Property of αH-tetradecachloro-4-nitrotriphenylmethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of αH-tetradecachloro-4-nitrotriphenylmethane

There total 1 articles about αH-tetradecachloro-4-nitrotriphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.4%

α-H,4-H-tetradecachlorotriphenylmethane (79839-44-4) → αH-tetradecachloro-4-nitrotriphenylmethane (82891-75-6)

Guidance literature:

With nitric acid; for 18h; Heating;

DOI:10.1021/jo00144a019

Reference yield: 93.3%

αH-tetradecachloro-4-nitrotriphenylmethane (82891-75-6) → αH-4-aminotetradecachlorotriphenylmethane (82891-74-5)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; In ethanol; for 120h; Heating;

DOI:10.1021/jo00144a019

Reference yield:

αH-tetradecachloro-4-nitrotriphenylmethane (82891-75-6) → 4-Aminotetradecachlorotriphenylmethyl Radical (64269-29-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 93.3 percent / SnCl₂*2H₂O, conc. aq. HCl / ethanol / 120 h / Heating

2: 1.) NaOH, 2.) I₂ / 1.) ether/Me₂SO, 48 h, 2.) 1 h

With hydrogenchloride; sodium hydroxide; iodine; tin(ll) chloride; In ethanol;

DOI:10.1021/jo00144a019

upstream raw materials:

α-H,4-H-tetradecachlorotriphenylmethane

Downstream raw materials:

αH-4-aminotetradecachlorotriphenylmethane

4-Aminotetradecachlorotriphenylmethyl Radical

4-<(chloroacetyl)amino>tetradecachlorotriphenylmethyl radical