4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol

Base Information

Chemical Name:4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol
CAS No.:863892-06-2
Molecular Formula:C₃₀H₃₉NO₈
Molecular Weight:541.642
Hs Code.:

Synonyms:4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol

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Chemical Property of 4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol

Chemical Property:

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Technology Process of 4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol

There total 6 articles about 4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 863892-02-8
1-O-(2-oxoethyl)-2,3:5,6-diisopropylidene-scyllo-inositol

: 863892-06-2
4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 76 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 12 h / 20 °C

2.1: 94 percent / silver(I) oxide; tetrabutylammonium iodide / CH₂Cl₂ / 12 h / 20 °C

3.1: NaOH / methanol / 12 h / 20 °C

3.2: 92 percent / aq. AcOH / methanol

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; silver(l) oxide; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/chem.200600898

Reference yield:

: 863892-01-7
4-O-allyl-1-O-benzoyl-2,3:5,6-di-O-isopropylidene-scyllo-inositol

: 863892-06-2
4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 92 percent / NaOMe / methanol / 3 h / Heating

2.1: 86 percent / sodium bicarbonate; ozone; triphenylphosphine / CH₂Cl₂; methanol / 12 h / 20 °C

3.1: 76 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 12 h / 20 °C

4.1: 94 percent / silver(I) oxide; tetrabutylammonium iodide / CH₂Cl₂ / 12 h / 20 °C

5.1: NaOH / methanol / 12 h / 20 °C

5.2: 92 percent / aq. AcOH / methanol

With sodium hydroxide; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; ozone; triphenylphosphine; silver(l) oxide; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/chem.200600898

Reference yield:

: 863892-03-9
1-O-(N,N-dibenzylaminoethyl)-2,3:5,6-diisopropylidene-scyllo-inositol

: 863892-06-2
4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 94 percent / silver(I) oxide; tetrabutylammonium iodide / CH₂Cl₂ / 12 h / 20 °C

2.1: NaOH / methanol / 12 h / 20 °C

2.2: 92 percent / aq. AcOH / methanol

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; silver(l) oxide; In methanol; dichloromethane;
DOI:10.1002/chem.200600898