5-(4-{[1-(3-isopropoxyphenyl)ethoxy]methyl}phenyl)-3-(methoxymethoxy)isoxazole

Base Information

Chemical Name:5-(4-{[1-(3-isopropoxyphenyl)ethoxy]methyl}phenyl)-3-(methoxymethoxy)isoxazole
CAS No.:1198745-21-9
Molecular Formula:C₂₃H₂₇NO₅
Molecular Weight:397.471
Hs Code.:

Synonyms:5-(4-{[1-(3-isopropoxyphenyl)ethoxy]methyl}phenyl)-3-(methoxymethoxy)isoxazole

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Chemical Property of 5-(4-{[1-(3-isopropoxyphenyl)ethoxy]methyl}phenyl)-3-(methoxymethoxy)isoxazole

Chemical Property:

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Technology Process of 5-(4-{[1-(3-isopropoxyphenyl)ethoxy]methyl}phenyl)-3-(methoxymethoxy)isoxazole

There total 6 articles about 5-(4-{[1-(3-isopropoxyphenyl)ethoxy]methyl}phenyl)-3-(methoxymethoxy)isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-52-5
nitromethane

: 1030828-94-4
4-[3-(methoxymethoxy)-1,2-oxazol-5-yl]phenol

: 114590-73-7
1-(3-isopropoxyphenyl)ethanone

: 1198745-21-9
5-(4-{[1-(3-isopropoxyphenyl)ethoxy]methyl}phenyl)-3-(methoxymethoxy)isoxazole

Guidance literature:: With triethylsilane; iron(III) chloride; Cooling with ice;

Reference yield:

: 1030828-96-6
5-[4-(benzyloxy)phenyl]-1,2-oxazol-3-ol

: 1198745-21-9
5-(4-{[1-(3-isopropoxyphenyl)ethoxy]methyl}phenyl)-3-(methoxymethoxy)isoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 20 °C

2: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol

3: triethylsilane / iron(III) chloride / Cooling with ice

With triethylsilane; hydrogen; triethylamine; iron(III) chloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol;

Reference yield:

: 540-38-5
p-Iodophenol

: 1198745-21-9
5-(4-{[1-(3-isopropoxyphenyl)ethoxy]methyl}phenyl)-3-(methoxymethoxy)isoxazole

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(I) oxide / N,N-dimethyl-formamide / 15 h / 110 °C

2.1: potassium carbonate / acetone / 4 h / 65 °C

3.1: hydroxylamine hydrochloride; potassium hydroxide / methanol / 20 °C

3.2: pH 2 - 3

4.1: triethylamine / tetrahydrofuran / 20 °C

5.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol

6.1: triethylsilane / iron(III) chloride / Cooling with ice

With copper(I) oxide; triethylsilane; hydroxylamine hydrochloride; hydrogen; potassium carbonate; triethylamine; potassium hydroxide; iron(III) chloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone;