2--N^α-(benzyloxycarbonyl)glycinyl>-2'-aminobenzoyl>pyridine

Base Information

• Chemical Name: 2--N^α-(benzyloxycarbonyl)glycinyl>-2'-aminobenzoyl>pyridine
• CAS No.: 153826-03-0
• Molecular Formula: C₂₇H₂₈N₄O₆
• Molecular Weight: 504.543

Synonyms:2--N^α-(benzyloxycarbonyl)glycinyl>-2'-aminobenzoyl>pyridine

Chemical Property of 2--N^α-(benzyloxycarbonyl)glycinyl>-2'-aminobenzoyl>pyridine

Chemical Property:

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Technology Process of 2--N^α-(benzyloxycarbonyl)glycinyl>-2'-aminobenzoyl>pyridine

There total 2 articles about 2--N^α-(benzyloxycarbonyl)glycinyl>-2'-aminobenzoyl>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-aminobenzoyl)pyridine (42471-56-7) + C20H28N2O8 → 2--Nα-(benzyloxycarbonyl)glycinyl>-2'-aminobenzoyl>pyridine (153826-03-0)

Guidance literature:

In dichloromethane; Yield given; 1.) 0 deg C, 0.5 h, 2.) RT, 4 h;

DOI:10.1021/jm00078a018

Reference yield:

α-<(tert-butyloxycarbonyl)amino>-Nα-(benzyloxycarbonyl)glycine (103711-23-5) → 2--Nα-(benzyloxycarbonyl)glycinyl>-2'-aminobenzoyl>pyridine (153826-03-0)

Guidance literature:

Multi-step reaction with 2 steps

1: N-methylmorpholine / CH₂Cl₂ / 0.5 h / 0 °C

2: CH₂Cl₂ / 1.) 0 deg C, 0.5 h, 2.) RT, 4 h

With 4-methyl-morpholine; In dichloromethane;

DOI:10.1021/jm00078a018

Reference yield:

2--Nα-(benzyloxycarbonyl)glycinyl>-2'-aminobenzoyl>pyridine (153826-03-0) → {Amino-[2-(pyridine-2-carbonyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester (1052665-90-3)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 23 ℃; for 0.166667h;

DOI:10.1021/jm00078a018

upstream raw materials:

2-(2-aminobenzoyl)pyridine

α-<(tert-butyloxycarbonyl)amino>-N^α-(benzyloxycarbonyl)glycine

Downstream raw materials:

{Amino-[2-(pyridine-2-carbonyl)-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester

1,3-dihydro-5-(pyridin-2-yl)-3(R,S)-[(benzyloxycarbonyl)-amino]-2H-1,4-benzodiazepin-2-one

(1-Methyl-2-oxo-5-pyridin-2-yl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)-carbamic acid benzyl ester

1,3-dihydro-1-(N,N-diethylacetamido)-5-(2-pyridyl)-3-(R,S)-<(benzyloxycarbonyl)amino>-2H-1,4-benzodiazepin-2-one

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