11-methoxy-11-phenyl-6-(3-(trifluoromethyl)phenyl)-11H-benzo[a]fluorene

Base Information

Chemical Name:11-methoxy-11-phenyl-6-(3-(trifluoromethyl)phenyl)-11H-benzo[a]fluorene
CAS No.:1620230-45-6
Molecular Formula:C₃₁H₂₁F₃O
Molecular Weight:466.502
Hs Code.:

Synonyms:11-methoxy-11-phenyl-6-(3-(trifluoromethyl)phenyl)-11H-benzo[a]fluorene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-methoxy-11-phenyl-6-(3-(trifluoromethyl)phenyl)-11H-benzo[a]fluorene

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Technology Process of 11-methoxy-11-phenyl-6-(3-(trifluoromethyl)phenyl)-11H-benzo[a]fluorene

There total 2 articles about 11-methoxy-11-phenyl-6-(3-(trifluoromethyl)phenyl)-11H-benzo[a]fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 59046-72-9
o-(phenylethynyl)benzaldehyde

: 126309-76-0
1-(2-phenylethynyl)-3-(trifluoromethyl)benzene

: 149-73-5
trimethyl orthoformate

: 1620230-45-6
11-methoxy-11-phenyl-6-(3-(trifluoromethyl)phenyl)-11H-benzo[a]fluorene

Guidance literature:: With trifluorormethanesulfonic acid; In acetonitrile; at 20 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c4cc03934c

Reference yield:

: 2-(2-phenylethynyl)benzaldehyde dimethylacetal

: 1620230-45-6
11-methoxy-11-phenyl-6-(3-(trifluoromethyl)phenyl)-11H-benzo[a]fluorene

Guidance literature:: Multi-step reaction with 2 steps

1: trifluorormethanesulfonic acid / acetonitrile / 24 h / 20 °C

2: trifluorormethanesulfonic acid / acetonitrile / 24 h / 20 °C / Inert atmosphere

With trifluorormethanesulfonic acid; In acetonitrile;
DOI:10.1039/c4cc03934c