N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine

Base Information

Chemical Name:N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine
CAS No.:830326-14-2
Molecular Formula:C₁₅H₁₆N₂O
Molecular Weight:240.305
Hs Code.:

Synonyms:N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine

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Chemical Property of N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine

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Technology Process of N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine

There total 1 articles about N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 3731-53-1
4-(aminomethyl)pyridine

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 830326-14-2
N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 4h; Heating;
DOI:10.1002/ejoc.200400460

Reference yield: 46.1%

: 75-15-0,12122-00-8
carbon disulfide

: 830326-14-2
N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine

: lithium 2-(4-methoxyphenyl)-2-methyl-4-(pyridin-4-yl)-5-thioxo-1,3-thiazolidine-3-ide

Guidance literature:: N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

carbon disulfide; In tetrahydrofuran; hexane; at -20 - 20 ℃; for 1h;
DOI:10.1002/ejoc.200500373

Reference yield: 46.1%

: 75-15-0,12122-00-8
carbon disulfide

: 830326-14-2
N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine

: lithium 2-(4-methoxyphenyl)-2-methyl-4-(pyridin-4-yl)-2,3-dihydro-1,3-thiazole-5-thiolate

Guidance literature:: N-[1-(4-methoxyphenyl)ethylidene]-(1-pyridin-4-yl)methanamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

carbon disulfide; In tetrahydrofuran; hexane; at -20 - 20 ℃; for 48h;
DOI:10.1002/ejoc.200500373