[Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]⁽¹⁺⁾*BF₄^(1-)*0.25CH₂Cl₂=[Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]BF₄*0.25CH₂Cl₂

Base Information

• Chemical Name: [Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]⁽¹⁺⁾*BF₄^(1-)*0.25CH₂Cl₂=[Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]BF₄*0.25CH₂Cl₂
• CAS No.: 96633-00-0
• Molecular Formula: BF₄*C₃₃H₂₅N₂O₄P₂Rh₂
• Molecular Weight: 889.369

Synonyms:[Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]⁽¹⁺⁾*BF₄^(1-)*0.25CH₂Cl₂=[Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]BF₄*0.25CH₂Cl₂

Chemical Property of [Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]⁽¹⁺⁾*BF₄^(1-)*0.25CH₂Cl₂=[Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]BF₄*0.25CH₂Cl₂

Chemical Property:

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Useful:

Technology Process of [Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]⁽¹⁺⁾*BF₄^(1-)*0.25CH₂Cl₂=[Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]BF₄*0.25CH₂Cl₂

There total 3 articles about [Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]⁽¹⁺⁾*BF₄^(1-)*0.25CH₂Cl₂=[Rh₂(CO)4(C₃HN₂(CH₂P(C₆H₅)2)2)]BF₄*0.25CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

[Rh2(C7H8)2(C3HN2(CH2P(C6H5)2)2)](1+)*BF4(1-)=[Rh2(C7H8)2(C3HN2(CH2P(C6H5)2)2)]BF4 (96532-18-2) → [Rh2(CO)4(C3HN2(CH2P(C6H5)2)2)](1+)*BF4(1-)*0.25CH2Cl2=[Rh2(CO)4(C3HN2(CH2P(C6H5)2)2)]BF4*0.25CH2Cl2 (96633-00-0)

Guidance literature:

With carbon monoxide; In dichloromethane; byproducts: norbornadiene; soln. of complex is treated with CO, further work-up under CO; addn. of hexane, recrystn. of ppt. from CH2Cl2/hexane, elem. anal.;

Reference yield: 100.0%

[Rh2(C8H12)2(C3HN2(CH2P(C6H5)2)2)](1+)*BF4(1-)*2CH3OH=[Rh2(C8H12)2(C3HN2(CH2P(C6H5)2)2)]BF4*2CH3OH (96616-78-3) → [Rh2(CO)4(C3HN2(CH2P(C6H5)2)2)](1+)*BF4(1-)*0.25CH2Cl2=[Rh2(CO)4(C3HN2(CH2P(C6H5)2)2)]BF4*0.25CH2Cl2 (96633-00-0)

Guidance literature:

With carbon monoxide; In dichloromethane; byproducts: 1,5-cyclooctadiene; soln. of complex is treated with CO, further work-up under CO; addn. of hexane, recrystn. of ppt. from CH2Cl2/hexane, elem. anal.;

Reference yield:

[(cod)Ir(3,5-bis((diphenylphosphino)methyl)pyrazolato)Rh(cod)]BF4 (881493-81-8) + carbon monoxide (201230-82-2) → [(CO)2Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Rh(CO)2]BF4 (96633-00-0) + [(CO)2Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)2]BF4 (881913-65-1) + [(CO)2Ir(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)2]BF4 (96616-80-7)

Guidance literature:

In dichloromethane; soln. Rh-Ir complex in CH2Cl2 was stirred under CO atm. (1 atm.) at roomtemp.;

DOI:10.1021/om050897e

upstream raw materials:

[Rh₂(C₇H₈)2(C₃HN₂(CH₂P(C₆H₅)2)2)]⁽¹⁺⁾*BF₄^(1-)=[Rh₂(C₇H₈)2(C₃HN₂(CH₂P(C₆H₅)2)2)]BF₄

[Rh₂(C₈H₁₂)2(C₃HN₂(CH₂P(C₆H₅)2)2)]⁽¹⁺⁾*BF₄^(1-)*2CH₃OH=[Rh₂(C₈H₁₂)2(C₃HN₂(CH₂P(C₆H₅)2)2)]BF₄*2CH₃OH

[(cod)Ir(3,5-bis((diphenylphosphino)methyl)pyrazolato)Rh(cod)]BF₄

carbon monoxide

Downstream raw materials:

[Rh₂(Cl)(CO)2(C₃HN₂(CH₂P(C₆H₅)2)2)]

[Rh₂(P(C₆H₅)2)(CO)2(C₃HN₂(CH₂P(C₆H₅)2)2)]

[(μ-η2:η2-HCC)Rh2(CO)2(3,5-bis(diphenylphosphino)methyl)pyrazolato)]

[(μ-η2:η2-(CH3)3SiCC)Rh2(CO)2(3,5-bis(diphenylphosphino)methyl)pyrazolato)]

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