C₂₇H₃₂⁽²⁾H₆O₇Si

Base Information

Chemical Name:C₂₇H₃₂⁽²⁾H₆O₇Si
CAS No.:1027914-76-6
Molecular Formula:C₂₇H₃₈O₇Si
Molecular Weight:508.632
Hs Code.:

C<sub>27</sub>H<sub>32</sub><sup>(2)</sup>H<sub>6</sub>O<sub>7</sub>Si

Synonyms:C₂₇H₃₂⁽²⁾H₆O₇Si

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₂⁽²⁾H₆O₇Si

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Technology Process of C₂₇H₃₂⁽²⁾H₆O₇Si

There total 10 articles about C₂₇H₃₂⁽²⁾H₆O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027570-63-3
C₃₄H₃₈⁽²⁾H₆O₇Si

: 1027914-76-6
C₂₇H₃₂⁽²⁾H₆O₇Si

Guidance literature:: With hydrogen; 10 percent Pd/C; In tetrahydrofuran; methanol; at 20 ℃; for 1h;
DOI:10.1039/b304411d

Reference yield:

: 4-hydroxy-3,5-di[²H₃]methoxybenzaldehyde

: 1027914-76-6
C₂₇H₃₂⁽²⁾H₆O₇Si

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / dimethylformamide / 4 h / 70 °C

2: NaBH₄ / methanol / 0.17 h / 20 °C

3: PBr₃ / diethyl ether / 1 h / 20 °C

4: lithium hexamethyldisilazanide / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.75 h / -35 °C

5: H₂ / 10 percent Pd/C / tetrahydrofuran; methanol / 1 h / 20 °C

With sodium tetrahydroborate; hydrogen; phosphorus tribromide; potassium carbonate; lithium hexamethyldisilazane; 10 percent Pd/C; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/b304411d

Reference yield:

: C₁₆H₁₂⁽²⁾H₆O₄

: 1027914-76-6
C₂₇H₃₂⁽²⁾H₆O₇Si

Guidance literature:: Multi-step reaction with 3 steps

1: PBr₃ / diethyl ether / 1 h / 20 °C

2: lithium hexamethyldisilazanide / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.75 h / -35 °C

3: H₂ / 10 percent Pd/C / tetrahydrofuran; methanol / 1 h / 20 °C

With hydrogen; phosphorus tribromide; lithium hexamethyldisilazane; 10 percent Pd/C; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1039/b304411d