methyl 2,6-di-tert-butylbenzoate

Base Information

Chemical Name:methyl 2,6-di-tert-butylbenzoate
CAS No.:1403387-19-8
Molecular Formula:C₁₆H₂₄O₂
Molecular Weight:248.365
Hs Code.:

Synonyms:methyl 2,6-di-tert-butylbenzoate

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Chemical Property of methyl 2,6-di-tert-butylbenzoate

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Technology Process of methyl 2,6-di-tert-butylbenzoate

There total 3 articles about methyl 2,6-di-tert-butylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 516526-99-1
2-bromo-1,3-bis(1-formyl-1-methylethyl)benzene

: 1403387-19-8
methyl 2,6-di-tert-butylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide; hydrazine hydrate / water; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol / 4 h / 120 - 200 °C

2.1: n-butyllithium / hexane; diethyl ether / 2 h / 20 °C / Inert atmosphere; Reflux

2.2: 2 h

3.1: diethyl ether / 20 °C

With n-butyllithium; hydrazine hydrate; potassium hydroxide; In diethyl ether; hexane; water; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; 1.1: Wolff-Kishner Reduction;

Reference yield:

: 19715-32-3
2-bromo-1,3-di-tert-butylbenzene

: 1403387-19-8
methyl 2,6-di-tert-butylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; diethyl ether / 2 h / 20 °C / Inert atmosphere; Reflux

1.2: 2 h

2.1: diethyl ether / 20 °C

With n-butyllithium; In diethyl ether; hexane;

Reference yield:

: 516526-98-0
2-bromo-1,3-bis(1-cyano-1-methylethyl)benzene

: 1403387-19-8
methyl 2,6-di-tert-butylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / toluene / 2 h / 0 - 20 °C / Inert atmosphere

1.2: 2 h

2.1: potassium hydroxide; hydrazine hydrate / water; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol / 4 h / 120 - 200 °C

3.1: n-butyllithium / hexane; diethyl ether / 2 h / 20 °C / Inert atmosphere; Reflux

3.2: 2 h

4.1: diethyl ether / 20 °C

With n-butyllithium; hydrazine hydrate; diisobutylaluminium hydride; potassium hydroxide; In diethyl ether; hexane; water; toluene; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; 2.1: Wolff-Kishner Reduction;