(1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol

Base Information

Chemical Name:(1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol
CAS No.:1338951-75-9
Molecular Formula:C₁₉H₂₈O₂
Molecular Weight:288.43
Hs Code.:

Synonyms:(1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol

Suppliers and Price of (1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol

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Technology Process of (1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol

There total 1 articles about (1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1245920-23-3
2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-one

: 1338951-75-9
(1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol

Guidance literature:: With dimethylsulfide borane complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at 0 ℃; for 1h; optical yield given as %ee; Inert atmosphere;
DOI:10.1016/j.tet.2011.08.050

Reference yield: 100.0%

: 1338951-75-9
(1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol

: 1338951-76-0
(1S,2S,6R)-1-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-6-methyl-7-oxabicyclo[4.1.0]heptan-2-ol

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h; optical yield given as %ee; Inert atmosphere;
DOI:10.1016/j.tet.2011.08.050

Reference yield:

: 1338951-75-9
(1S)-2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-ol

: 1338951-77-1
C₁₉H₂₆O₃

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 2: Dess-Martin oxidation;
DOI:10.1016/j.tet.2011.08.050