N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine

Base Information

• Chemical Name: N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine
• CAS No.: 1031794-89-4
• Molecular Formula: C₁₈H₂₁N₃OS
• Molecular Weight: 327.45
• Mol file: 1031794-89-4.mol

Synonyms:N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine

Chemical Property of N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine

There total 1 articles about N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[(diethylamino)carbonothioyl]benzenecarboximidoyl chloride (82655-59-2) + 2-amino-phenol (95-55-6) → N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine (1031794-89-4)

Guidance literature:

With triethylamine; In acetone;

DOI:10.1002/aoc.3652

Reference yield: 87.0%

tetra-n-butylammonium tetrachlorooxorhenate(V) + N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine (1031794-89-4) → (N-[(diethylamino)(thiocarbonyl)]benzimidinato)chloridooxidorhenium(V)

Guidance literature:

In methanol; a soln. of ligand added dropwise to a soln. of Re complex, reacted for 30 min; filtered off, washed (cold MeOH), recrystd. (CH2Cl2/MeOH); elem. anal.;

DOI:10.1021/ic702344s

Reference yield: 86.0%

tetrabutylammonium [(99g)Tc]tetrachlorooxotechnetate(V) + N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine (1031794-89-4) → [(99)TcO(N-(N'',N''-diethylaminothiocarbonyl)-N'-(2-hydroxyphenyl)benzamidine(-2H))Cl]

Guidance literature:

In methanol; a soln. of ligand added dropwise to a soln. of (99)Tc complex; filtered off, washed (cold MeOH); elem. anal.;

DOI:10.1021/ic702344s

upstream raw materials:

N-[(diethylamino)carbonothioyl]benzenecarboximidoyl chloride

2-amino-phenol