di(tert-butyl) [6-(benzyloxy)-9-(prop-2-yn-1-yl)-9H-purin-2-yl]imidodicarbonate

Base Information

Chemical Name:di(tert-butyl) [6-(benzyloxy)-9-(prop-2-yn-1-yl)-9H-purin-2-yl]imidodicarbonate
CAS No.:1421193-80-7
Molecular Formula:C₂₅H₂₉N₅O₅
Molecular Weight:479.536
Hs Code.:

Synonyms:di(tert-butyl) [6-(benzyloxy)-9-(prop-2-yn-1-yl)-9H-purin-2-yl]imidodicarbonate

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Chemical Property of di(tert-butyl) [6-(benzyloxy)-9-(prop-2-yn-1-yl)-9H-purin-2-yl]imidodicarbonate

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Technology Process of di(tert-butyl) [6-(benzyloxy)-9-(prop-2-yn-1-yl)-9H-purin-2-yl]imidodicarbonate

There total 6 articles about di(tert-butyl) [6-(benzyloxy)-9-(prop-2-yn-1-yl)-9H-purin-2-yl]imidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1421193-78-3
di(tert-butyl) [6-(benzyloxy)-9H-purin-2-yl]imidodicarbonate

: 106-96-7
propargyl bromide

: 1421193-80-7
di(tert-butyl) [6-(benzyloxy)-9-(prop-2-yn-1-yl)-9H-purin-2-yl]imidodicarbonate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; toluene; at 20 ℃; for 15h;
DOI:10.1002/hlca.201200557

Reference yield:

: 1384872-38-1
tert-butyl 6-(benzyloxy)-2-{[bis(tert-butoxy)carbonyl]amino}-9H-purine-9-carboxylate

: 1421193-80-7
di(tert-butyl) [6-(benzyloxy)-9-(prop-2-yn-1-yl)-9H-purin-2-yl]imidodicarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / methanol; water / 1 h / 50 °C

2: potassium carbonate / N,N-dimethyl-formamide; toluene / 15 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In methanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.201200557

Reference yield:

: 19916-73-5
2-Amino-6-benzyloxypurine

: 1421193-80-7
di(tert-butyl) [6-(benzyloxy)-9-(prop-2-yn-1-yl)-9H-purin-2-yl]imidodicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / tetrahydrofuran / 15 h / 20 °C

2: sodium hydrogencarbonate / methanol; water / 1 h / 50 °C

3: potassium carbonate / N,N-dimethyl-formamide; toluene / 15 h / 20 °C

With dmap; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.201200557