methyl 4-((3-((2,6-dimethylmorpholino)methyl)-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

Base Information

Chemical Name:methyl 4-((3-((2,6-dimethylmorpholino)methyl)-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate
CAS No.:1432509-43-7
Molecular Formula:C₂₈H₃₂N₂O₄
Molecular Weight:460.573
Hs Code.:

Synonyms:methyl 4-((3-((2,6-dimethylmorpholino)methyl)-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

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Chemical Property of methyl 4-((3-((2,6-dimethylmorpholino)methyl)-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

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Technology Process of methyl 4-((3-((2,6-dimethylmorpholino)methyl)-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

There total 4 articles about methyl 4-((3-((2,6-dimethylmorpholino)methyl)-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 141-91-3
2,6-dimethyl morpholine

: 1432509-37-9
methyl 4-((3-methylen-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

: 1432509-43-7
methyl 4-((3-((2,6-dimethylmorpholino)methyl)-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

Guidance literature:: In toluene; at 110 ℃; for 1.5h; Microwave irradiation;

Reference yield:

: 100-63-0
phenylhydrazine

: 1432509-43-7
methyl 4-((3-((2,6-dimethylmorpholino)methyl)-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / 0.17 h / 140 °C / Microwave irradiation

2.1: sodium hydride / N,N-dimethyl-formamide; paraffin oil / 0.17 h

2.2: 5 h / 50 °C

3.1: N,N-dimethylammonium chloride; acetic acid / toluene / 4 h / 100 °C

3.2: 12 h / 80 °C

4.1: toluene / 1.5 h / 110 °C / Microwave irradiation

With N,N-dimethylammonium chloride; sodium hydride; acetic acid; trifluoroacetic acid; In N,N-dimethyl-formamide; toluene; paraffin oil; 1.1: |Fischer Indole Synthesis;

Reference yield:

: 15128-52-6
1,2,3,9-tetrahydro-4H-carbazol-4-one

: 1432509-43-7
methyl 4-((3-((2,6-dimethylmorpholino)methyl)-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; paraffin oil / 0.17 h

1.2: 5 h / 50 °C

2.1: N,N-dimethylammonium chloride; acetic acid / toluene / 4 h / 100 °C

2.2: 12 h / 80 °C

3.1: toluene / 1.5 h / 110 °C / Microwave irradiation

With N,N-dimethylammonium chloride; sodium hydride; acetic acid; In N,N-dimethyl-formamide; toluene; paraffin oil;