ethanolN--Ala-Pro-OEt

Base Information

Chemical Name:ethanolN--Ala-Pro-OEt
CAS No.:94670-65-2
Molecular Formula:C₂₅H₃₅N₃O₆
Molecular Weight:473.569
Hs Code.:

ethanolN-<carboethoxy(N-benzoyl-2-pyrrolidinyl)methyl>-Ala-Pro-OEt

Synonyms:ethanolN--Ala-Pro-OEt

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethanolN--Ala-Pro-OEt

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Technology Process of ethanolN--Ala-Pro-OEt

There total 6 articles about ethanolN--Ala-Pro-OEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 93-97-0
benzoic acid anhydride

: 94670-66-3
N-methyl>-Ala-Pro-OEt

: 94670-65-2
ethanolN--Ala-Pro-OEt

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/jm00382a008

Reference yield:

: 13485-59-1
L-alanyl-L-proline

: 94670-65-2
ethanolN--Ala-Pro-OEt

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / 96 h

2: 1.) HCl, 2.) di-tert-butyldicarbonate, triethylamine / 1.) RT, 4 d, 2.) 24 h

3: 42 percent / Amberlyst XN-1010 acidic resin / 216 h / 70 °C

4: 55 percent / triethylamine / CH₂Cl₂

With hydrogenchloride; di-tert-butyl dicarbonate; Amberlyst XN-1010 acidic resin; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm00382a008

Reference yield:

: 59936-29-7
(S)-N-(tert-butoxycarbonyl)proline methyl ester

: 94670-65-2
ethanolN--Ala-Pro-OEt

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminum hydride / toluene; hexane / 0.5 h

2: methanol / 96 h

3: 1.) HCl, 2.) di-tert-butyldicarbonate, triethylamine / 1.) RT, 4 d, 2.) 24 h

4: 42 percent / Amberlyst XN-1010 acidic resin / 216 h / 70 °C

5: 55 percent / triethylamine / CH₂Cl₂

With hydrogenchloride; di-tert-butyl dicarbonate; Amberlyst XN-1010 acidic resin; diisobutylaluminium hydride; triethylamine; In methanol; hexane; dichloromethane; toluene;
DOI:10.1021/jm00382a008