2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside
CAS No.:1277151-59-3
Molecular Formula:C₅₀H₅₃BrF₁₇O₁₀PSi
Molecular Weight:1275.9
Hs Code.:

2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside

Synonyms:2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside

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Chemical Property of 2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside

There total 6 articles about 2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₀H₅₃BrF₁₇O₉PSi

: 1277151-59-3
2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside

Guidance literature:: With tert.-butylhydroperoxide; In nonane; dichloromethane; acetonitrile; Inert atmosphere;
DOI:10.1021/ol2003435

Reference yield:

: 89807-86-3
2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-1-ol

: 1277151-59-3
2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole / tetrahydrofuran; dichloromethane / 20 °C / Inert atmosphere

2: 1H-tetrazole / dichloromethane; acetonitrile / 20 °C / Inert atmosphere

3: tert.-butylhydroperoxide / nonane; dichloromethane; acetonitrile / Inert atmosphere

With 1H-tetrazole; tert.-butylhydroperoxide; In tetrahydrofuran; nonane; dichloromethane; acetonitrile;
DOI:10.1021/ol2003435

Reference yield:

: 1277151-49-1
benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl diisopropylphosphoramidite

: 1277151-59-3
2-(trimethylsilyl)ethyl 2,4-di-O-benzyl-6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-3-O-p-methoxybenzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / dichloromethane; acetonitrile / 20 °C / Inert atmosphere

2: tert.-butylhydroperoxide / nonane; dichloromethane; acetonitrile / Inert atmosphere

With 1H-tetrazole; tert.-butylhydroperoxide; In nonane; dichloromethane; acetonitrile;
DOI:10.1021/ol2003435