7-(4-chlorophenyl)-9-(4-methoxyphenyl)-1,4-diazaspiro[4.5]deca-9-ene-6-ethyl carboxylate

Base Information

Chemical Name:7-(4-chlorophenyl)-9-(4-methoxyphenyl)-1,4-diazaspiro[4.5]deca-9-ene-6-ethyl carboxylate
CAS No.:1290640-01-5
Molecular Formula:C₂₄H₂₇ClN₂O₃
Molecular Weight:426.943
Hs Code.:

Synonyms:7-(4-chlorophenyl)-9-(4-methoxyphenyl)-1,4-diazaspiro[4.5]deca-9-ene-6-ethyl carboxylate

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Chemical Property of 7-(4-chlorophenyl)-9-(4-methoxyphenyl)-1,4-diazaspiro[4.5]deca-9-ene-6-ethyl carboxylate

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Technology Process of 7-(4-chlorophenyl)-9-(4-methoxyphenyl)-1,4-diazaspiro[4.5]deca-9-ene-6-ethyl carboxylate

There total 4 articles about 7-(4-chlorophenyl)-9-(4-methoxyphenyl)-1,4-diazaspiro[4.5]deca-9-ene-6-ethyl carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1245938-53-7
C₂₂H₂₁ClO₄

: 107-15-3,85404-18-8
ethylenediamine

: 1290640-01-5
7-(4-chlorophenyl)-9-(4-methoxyphenyl)-1,4-diazaspiro[4.5]deca-9-ene-6-ethyl carboxylate

Guidance literature:: With toluene-4-sulfonic acid; at 120 ℃; under 3000.3 Torr; Microwave irradiation; neat (no solvent);
DOI:10.1007/s10593-011-0801-5

Reference yield:

: 6552-68-7
4-chloro-4'-methoxy-chalcone

: 1290640-01-5
7-(4-chlorophenyl)-9-(4-methoxyphenyl)-1,4-diazaspiro[4.5]deca-9-ene-6-ethyl carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium ethanolate / ethanol / 2 h / Reflux

2: activated fly ash / 0.1 h / 90 °C / 1500.15 Torr / Microwave irradiation

With sodium ethanolate; In ethanol;
DOI:10.3109/14756366.2010.503611

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1290640-01-5
7-(4-chlorophenyl)-9-(4-methoxyphenyl)-1,4-diazaspiro[4.5]deca-9-ene-6-ethyl carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 1 h / 20 °C

2: sodium ethanolate / ethanol / 2 h / Reflux

3: activated fly ash / 0.1 h / 90 °C / 1500.15 Torr / Microwave irradiation

With sodium ethanolate; sodium hydroxide; In ethanol;
DOI:10.3109/14756366.2010.503611