C₄₄H₅₉N₃O₅

Base Information

Chemical Name:C₄₄H₅₉N₃O₅
CAS No.:1351815-80-9
Molecular Formula:C₄₄H₅₉N₃O₅
Molecular Weight:709.97
Hs Code.:

C<sub>44</sub>H<sub>59</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₄₄H₅₉N₃O₅

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Chemical Property of C₄₄H₅₉N₃O₅

Chemical Property:

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Technology Process of C₄₄H₅₉N₃O₅

There total 9 articles about C₄₄H₅₉N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 912545-08-5
2,4-bis-benzyloxy-5-isopropenyl-benzoic acid methyl ester

: 1351815-80-9
C₄₄H₅₉N₃O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide; methanol / 20 h / 75 °C

1.2: 0.5 h / 20 °C

2.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 36 h / 20 °C

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1.5 h / 20 °C / Molecular sieve

4.1: sodium tris(acetoxy)borohydride / 2 h / Inert atmosphere

With methanol; tetrapropylammonium perruthennate; sodium tris(acetoxy)borohydride; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In dichloromethane;

Reference yield:

: 1351815-89-8
cyclopentyl N-(3-aminopropyl)-L-leucinate

: 1351815-41-2
1-{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}piperidine-4-carbaldehyde

: 1351815-80-9
C₄₄H₅₉N₃O₅

Guidance literature:: cyclopentyl N-(3-aminopropyl)-L-leucinate; 1-{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}piperidine-4-carbaldehyde; With sodium tris(acetoxy)borohydride; for 2h; Inert atmosphere;

With water; In dichloromethane;

Reference yield:

: 2150-47-2
methyl 2,4-dihydroxybenzoate

: 1351815-80-9
C₄₄H₅₉N₃O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap / 1 h / 55 °C

2.1: trifluorormethanesulfonic acid / toluene / 2.5 h / 20 °C / Cooling with ice

2.2: 18 h / 20 °C

3.1: potassium carbonate / acetonitrile / 42 h / 75 °C

4.1: potassium tert-butylate / tetrahydrofuran / 0.5 h

4.2: 0.5 h

5.1: potassium hydroxide; methanol / 20 h / 75 °C

5.2: 0.5 h / 20 °C

6.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 36 h / 20 °C

7.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1.5 h / 20 °C / Molecular sieve

8.1: sodium tris(acetoxy)borohydride / 2 h / Inert atmosphere

With methanol; tetrapropylammonium perruthennate; trifluorormethanesulfonic acid; potassium tert-butylate; sodium tris(acetoxy)borohydride; potassium carbonate; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; dmap; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;