1,1-Di-(4-methoxyphenyl)-1-[4-(1H,1H,2H,2H-perfluorodecyl)phenyl]methyl chloride

Base Information

• Chemical Name: 1,1-Di-(4-methoxyphenyl)-1-[4-(1H,1H,2H,2H-perfluorodecyl)phenyl]methyl chloride
• CAS No.: 865758-36-7
• Molecular Formula: C31H22 Cl F17 O2
• Molecular Weight: 784.93
• European Community (EC) Number: 623-168-2
• DSSTox Substance ID: DTXSID00468500
• Wikidata: Q82295721
• Mol file: 865758-36-7.mol

Synonyms:865758-36-7;1,1-Di-(4-methoxyphenyl)-1-[4-(1H,1H,2H,2H-perfluorodecyl)phenyl]methyl chloride;1-[chloro-bis(4-methoxyphenyl)methyl]-4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzene;SCHEMBL6040882;DTXSID00468500;NS00019290;1,1-Di-(4-methoxyphenyl)-1-(4-(1H,1H,2H,2H-perfluorodecyl)phenyl)methyl chloride,98%;1,1-Di-(4-methoxyphenyl)-1-[4-(1H,1H,2H,2H-perfluorodecyl)phenyl]methyl chloride, >=90%;1,1'-{Chloro[4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl]methylene}bis(4-methoxybenzene)

Chemical Property of 1,1-Di-(4-methoxyphenyl)-1-[4-(1H,1H,2H,2H-perfluorodecyl)phenyl]methyl chloride

Chemical Property:

• Melting Point: 131-137°C
• PSA: 18.46000
• LogP: 11.17650
• XLogP3: 11.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 19
• Rotatable Bond Count: 14
• Exact Mass: 784.1036864
• Heavy Atom Count: 51
• Complexity: 1110

Purity/Quality:

98%Min ^*data from raw suppliers

1,1-DI-(4-METHOXYPHENYL)-1-[4-(1H,1H,2H,2H-PERFLUORODECYL)PHENYL]METHYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C(C2=CC=C(C=C2)CCC(C(C(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(C3=CC=C(C=C3)OC)Cl

Technology Process of 1,1-Di-(4-methoxyphenyl)-1-[4-(1H,1H,2H,2H-perfluorodecyl)phenyl]methyl chloride

There total 3 articles about 1,1-Di-(4-methoxyphenyl)-1-[4-(1H,1H,2H,2H-perfluorodecyl)phenyl]methyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'dimethoxy-4''-[4-(1H,1H,2H,2H)-perfluorodecyl]trityl alcohol (865758-47-0) → 4,4'dimethoxy-4''-(1H,1H,2H,2H-perfluorodecyl)trityl chloride (865758-36-7)

Guidance literature:

With acetyl chloride; In cyclohexane; for 1h; Heating;

DOI:10.1021/jo050795y

Reference yield:

4-methoxyphenyl magnesium bromide (13139-86-1) → 4,4'dimethoxy-4''-(1H,1H,2H,2H-perfluorodecyl)trityl chloride (865758-36-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h

2: 4.08 g / acetyl chloride / cyclohexane / 1 h / Heating

With acetyl chloride; In tetrahydrofuran; cyclohexane;

DOI:10.1021/jo050795y

Reference yield:

methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzoate (495388-45-9) → 4,4'dimethoxy-4''-(1H,1H,2H,2H-perfluorodecyl)trityl chloride (865758-36-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h

2: 4.08 g / acetyl chloride / cyclohexane / 1 h / Heating

With acetyl chloride; In tetrahydrofuran; cyclohexane;

DOI:10.1021/jo050795y

upstream raw materials:

4,4'dimethoxy-4''-[4-(1H,1H,2H,2H)-perfluorodecyl]trityl alcohol

4-methoxyphenyl magnesium bromide

methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzoate

Downstream raw materials:

5'-O-[4,4'-dimethoxy-4''-(1H,1H,2H,2H-perfluorodecyl)trityl]thymidine

N⁶-benzoyl-5'-O-[4,4'-dimethoxy-4''-(1H,1H,2H,2H-perfluorodecyl)trityl]-2'-deoxyadenosine

N⁴-benzoyl-5'-O-[4,4'-dimethoxy-4''-(1H,1H,2H,2H-perfluorodecyl)trityl]-2'-deoxycytidine

5'-O-[4,4'-dimethoxy-4''-(1H,1H,2H,2H-perfluorodecyl)trityl]-N²-isobutyryl-2'-deoxyguanosine

Refernces