5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

Base Information

Chemical Name:5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine
CAS No.:132018-98-5
Molecular Formula:C₄₂H₄₉N₁₁O₂₆P₂
Molecular Weight:1185.86
Hs Code.:

5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-<N-(6-nitroveratryloxycarbonyl)-γ-(O-6-nitroveratryl)-L-aspartyl>adenosine

Synonyms:5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

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Chemical Property of 5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

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Technology Process of 5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

There total 4 articles about 5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1016-58-6
6-nitroveratryl alcohol

: 132018-98-5
5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / dicyclohexylcarbodiimide (DCC), (dimethylamino)pyridine / CH₂Cl₂ / 2 h / Ambient temperature

2: CF₃CO₂H, p-dimethoxybenzene / CH₂Cl₂ / 5 h / Ambient temperature

3: Et₃N / acetonitrile / Ambient temperature

4: 1.) Dowex 1x8-200 ion-exchange beads (Bu₄N-form), Bu₄NOH / 1.) H₂O, 2.) DMF, RT, 2.5 h

With dmap; Dowex 1x8-200 ion-exchange beads (Bu₄N-form); tetra(n-butyl)ammonium hydroxide; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; 1,4-dimethoxybezene; In dichloromethane; acetonitrile;
DOI:10.1021/ja00007a055

Reference yield:

: (S)-2-Amino-succinic acid 4-(4,5-dimethoxy-2-nitro-benzyl) ester

: 132018-98-5
5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / acetonitrile / Ambient temperature

2: 1.) Dowex 1x8-200 ion-exchange beads (Bu₄N-form), Bu₄NOH / 1.) H₂O, 2.) DMF, RT, 2.5 h

With Dowex 1x8-200 ion-exchange beads (Bu₄N-form); tetra(n-butyl)ammonium hydroxide; triethylamine; In acetonitrile;
DOI:10.1021/ja00007a055

Reference yield:

: 132018-90-7
N-Boc-L-aspartic acid α-tert-butyl β-6-nitroveratryl diester

: 132018-98-5
5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

Guidance literature:: Multi-step reaction with 3 steps

1: CF₃CO₂H, p-dimethoxybenzene / CH₂Cl₂ / 5 h / Ambient temperature

2: Et₃N / acetonitrile / Ambient temperature

3: 1.) Dowex 1x8-200 ion-exchange beads (Bu₄N-form), Bu₄NOH / 1.) H₂O, 2.) DMF, RT, 2.5 h

With Dowex 1x8-200 ion-exchange beads (Bu₄N-form); tetra(n-butyl)ammonium hydroxide; triethylamine; trifluoroacetic acid; 1,4-dimethoxybezene; In dichloromethane; acetonitrile;
DOI:10.1021/ja00007a055