7-BROMO-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE

Base Information

• Chemical Name: 7-BROMO-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE
• CAS No.: 865472-04-4
• Molecular Formula: C₁₀H₁₂BrN
• Molecular Weight: 226.116
• Hs Code.: 2921450090
• Mol file: 865472-04-4.mol

Synonyms:7-BROMO-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE;7-bromo-1,2,3,4-tetrahydronaphthalen-1-amine;7-bromo-1,2,3,4-tetrahydronaphthalen-1-amine hydrochloride

Chemical Property of 7-BROMO-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE

Chemical Property:

• PSA: 26.02000
• LogP: 3.48550

Purity/Quality:

99%, ^*data from raw suppliers

7-Bromo-1,2,3,4-tetrahydro-naphthalen-1-ylamine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-BROMO-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE

There total 2 articles about 7-BROMO-1,2,3,4-TETRAHYDRO-NAPHTHALEN-1-YLAMINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

bromo-7 dihydro-3,4 naphthalene (75693-17-3) → (+/-)-1-amino-7-bromo-1,2,3,4-tetrahydronaphthalene (794507-89-4,865472-04-4)

Guidance literature:

With ammonium acetate; sodium cyanoborohydride; In ethanol; at 130 ℃; for 0.0333333h; Microwave irradiation;

Reference yield: 81.0%

7-bromo-3,4-dihydro-2H-naphthalen-1-one (32281-97-3) → (+/-)-1-amino-7-bromo-1,2,3,4-tetrahydronaphthalene (794507-89-4,865472-04-4)

Guidance literature:

With ammonium acetate; sodium cyanoborohydride; In ethanol; at 130 ℃; for 0.0333333h; Microwave irradiation;

DOI:10.1016/j.tetlet.2010.07.156

upstream raw materials:

7-bromo-3,4-dihydro-2H-naphthalen-1-one

bromo-7 dihydro-3,4 naphthalene

Refernces

• 1、 Dong, Li,Aleem, Saadat,Fink, Cynthia A.. "Microwave-accelerated reductive amination between ketones and ammonium acetate". experimental part. p. 5210 - 5212. Retrieved 2010/11/05.