(N-(pyren-1-ylmethyl)-N-(benzyl-2-boronic acid)-aminoethyl) (N'-(4-(azidomethyl)benzyl)-N'-(benzyl-2'-boronic acid)-3-aminopropyl)ether

Base Information

Chemical Name:(N-(pyren-1-ylmethyl)-N-(benzyl-2-boronic acid)-aminoethyl) (N'-(4-(azidomethyl)benzyl)-N'-(benzyl-2'-boronic acid)-3-aminopropyl)ether
CAS No.:1385773-96-5
Molecular Formula:C₄₄H₄₅B₂N₅O₅
Molecular Weight:745.494
Hs Code.:

Synonyms:(N-(pyren-1-ylmethyl)-N-(benzyl-2-boronic acid)-aminoethyl) (N'-(4-(azidomethyl)benzyl)-N'-(benzyl-2'-boronic acid)-3-aminopropyl)ether

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Chemical Property of (N-(pyren-1-ylmethyl)-N-(benzyl-2-boronic acid)-aminoethyl) (N'-(4-(azidomethyl)benzyl)-N'-(benzyl-2'-boronic acid)-3-aminopropyl)ether

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Technology Process of (N-(pyren-1-ylmethyl)-N-(benzyl-2-boronic acid)-aminoethyl) (N'-(4-(azidomethyl)benzyl)-N'-(benzyl-2'-boronic acid)-3-aminopropyl)ether

There total 13 articles about (N-(pyren-1-ylmethyl)-N-(benzyl-2-boronic acid)-aminoethyl) (N'-(4-(azidomethyl)benzyl)-N'-(benzyl-2'-boronic acid)-3-aminopropyl)ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1385773-95-4
2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

: potassium (2-formylphenyl)trifluoroborate

: 1385773-96-5
(N-(pyren-1-ylmethyl)-N-(benzyl-2-boronic acid)-aminoethyl) (N'-(4-(azidomethyl)benzyl)-N'-(benzyl-2'-boronic acid)-3-aminopropyl)ether

Guidance literature:: 2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether; potassium (2-formylphenyl)trifluoroborate; With sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 72h; Inert atmosphere;

With sodium tetrahydroborate; In tetrahydrofuran;

With water; lithium hydroxide; In acetonitrile; at 20 ℃;

Reference yield:

: 1385773-92-1
2-(t-butoxycarbonylamino)ethyl 3-(benzyloxycarbonylamino)propyl ether

: 1385773-96-5
(N-(pyren-1-ylmethyl)-N-(benzyl-2-boronic acid)-aminoethyl) (N'-(4-(azidomethyl)benzyl)-N'-(benzyl-2'-boronic acid)-3-aminopropyl)ether

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen; ammonia / palladium on activated charcoal / tetrahydrofuran; methanol / 1 h / 760.05 Torr

2.1: methanol

3.1: sodium tetrahydroborate; methanol / 2 h / 0 °C

4.1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

5.1: tetrahydrofuran; methanol

6.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 1 h / 0 °C

7.1: N-ethyl-N,N-diisopropylamine; sodium tris(acetoxy)borohydride / tetrahydrofuran / 72 h / Inert atmosphere

7.3: 20 °C

With methanol; sodium tetrahydroborate; ammonia; hydrogen; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 125734-44-3
4-(hydroxymethyl)benzaldehyde diethyl acetal

: 1385773-96-5
(N-(pyren-1-ylmethyl)-N-(benzyl-2-boronic acid)-aminoethyl) (N'-(4-(azidomethyl)benzyl)-N'-(benzyl-2'-boronic acid)-3-aminopropyl)ether

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 1 h

2.1: hydrogen bromide / dichloromethane; acetic acid

3.1: sodium azide / N,N-dimethyl-formamide / 1 h / 60 °C

4.1: methanol

5.1: sodium tetrahydroborate; methanol / 2 h / 0 °C

6.1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

7.1: tetrahydrofuran; methanol

8.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 1 h / 0 °C

9.1: N-ethyl-N,N-diisopropylamine; sodium tris(acetoxy)borohydride / tetrahydrofuran / 72 h / Inert atmosphere

9.3: 20 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; sodium azide; water; hydrogen bromide; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;