2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

Base Information

Chemical Name:2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether
CAS No.:1385773-95-4
Molecular Formula:C₃₀H₃₁N₅O
Molecular Weight:477.609
Hs Code.:

Synonyms:2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

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Chemical Property of 2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

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Technology Process of 2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

There total 11 articles about 2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₂₉N₅O

: 1385773-95-4
2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

Guidance literature:: With methanol; sodium tetrahydroborate; In tetrahydrofuran; at 0 ℃; for 1h;

Reference yield:

: 1385773-92-1
2-(t-butoxycarbonylamino)ethyl 3-(benzyloxycarbonylamino)propyl ether

: 1385773-95-4
2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogen; ammonia / palladium on activated charcoal / tetrahydrofuran; methanol / 1 h / 760.05 Torr

2: methanol

3: sodium tetrahydroborate; methanol / 2 h / 0 °C

4: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

5: tetrahydrofuran; methanol

6: sodium tetrahydroborate; methanol / tetrahydrofuran / 1 h / 0 °C

With methanol; sodium tetrahydroborate; ammonia; hydrogen; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 125734-44-3
4-(hydroxymethyl)benzaldehyde diethyl acetal

: 1385773-95-4
2-(pyren-1-ylmethylamino)ethyl 3-N-(4-(azidomethyl)benzyl)-aminopropyl ether

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride; water / tetrahydrofuran / 1 h

2: hydrogen bromide / dichloromethane; acetic acid

3: sodium azide / N,N-dimethyl-formamide / 1 h / 60 °C

4: methanol

5: sodium tetrahydroborate; methanol / 2 h / 0 °C

6: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

7: tetrahydrofuran; methanol

8: sodium tetrahydroborate; methanol / tetrahydrofuran / 1 h / 0 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; sodium azide; water; hydrogen bromide; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;