Pentanedioic acid, 3-phenyl-, monobutyl ester, (3S)- (9CI)

Base Information

Chemical Name:Pentanedioic acid, 3-phenyl-, monobutyl ester, (3S)- (9CI)
CAS No.:865366-96-7
Molecular Formula:C15H20 O4
Molecular Weight:264.321
Hs Code.:
Mol file:865366-96-7.mol

Synonyms:Pentanedioicacid, 3-phenyl-, monobutyl ester, (3S)- (9CI)

Suppliers and Price of Pentanedioic acid, 3-phenyl-, monobutyl ester, (3S)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Pentanedioic acid, 3-phenyl-, monobutyl ester, (3S)- (9CI)

Chemical Property:

Melting Point:41-43 °C(Solv: ethyl ether (60-29-7); hexane (110-54-3))
Boiling Point:400.4±33.0 °C(Predicted)
PKA:4.44±0.10(Predicted)
PSA：63.60000
Density:1.116±0.06 g/cm3(Predicted)
LogP:2.97830

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Pentanedioic acid, 3-phenyl-, monobutyl ester, (3S)- (9CI)

There total 3 articles about Pentanedioic acid, 3-phenyl-, monobutyl ester, (3S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4160-80-9
3-phenylglutaric acid anhydride

: 71-36-3
butan-1-ol

: (R)-3-phenylglutaric acid monobutyl ester

: 865366-96-7
(S)-3-phenylglutaric acid monobutyl ester

Guidance literature:: With Novozym 435; In di-isopropyl ether; at 20 ℃; for 408h; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2005.06.025

Reference yield:

: 4165-96-2
3-phenylglutaric acid

: 865366-96-7
(S)-3-phenylglutaric acid monobutyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: AcCl / 3 h

2: Novozym 435 / diisopropyl ether / 408 h / 20 °C

With Novozym 435; acetyl chloride; In di-isopropyl ether;
DOI:10.1016/j.tetasy.2005.06.025

Reference yield:

: 100-52-7
benzaldehyde

: 865366-96-7
(S)-3-phenylglutaric acid monobutyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine / 72 h / 20 °C

1.2: aq. KOH / 3 h / 80 - 95 °C

2.1: AcCl / 3 h

3.1: Novozym 435 / diisopropyl ether / 408 h / 20 °C

With piperidine; Novozym 435; acetyl chloride; In di-isopropyl ether;
DOI:10.1016/j.tetasy.2005.06.025