Thiocarbonic acid O-{4-[bis-(2-chloro-ethyl)-amino]-phenyl} ester O-pentafluorophenyl ester

Base Information

Chemical Name:Thiocarbonic acid O-{4-[bis-(2-chloro-ethyl)-amino]-phenyl} ester O-pentafluorophenyl ester
CAS No.:174579-29-4
Molecular Formula:C₁₇H₁₂Cl₂F₅NO₂S
Molecular Weight:460.252
Hs Code.:

Synonyms:Thiocarbonic acid O-{4-[bis-(2-chloro-ethyl)-amino]-phenyl} ester O-pentafluorophenyl ester

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Chemical Property of Thiocarbonic acid O-{4-[bis-(2-chloro-ethyl)-amino]-phenyl} ester O-pentafluorophenyl ester

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Technology Process of Thiocarbonic acid O-{4-[bis-(2-chloro-ethyl)-amino]-phenyl} ester O-pentafluorophenyl ester

There total 5 articles about Thiocarbonic acid O-{4-[bis-(2-chloro-ethyl)-amino]-phenyl} ester O-pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1204-69-9
4-[bis(2-chloroethyl)amino]phenol

: 135192-53-9
pentafluorophenoxythiocarbonyl chloride

: 174579-29-4
Thiocarbonic acid O-{4-[bis-(2-chloro-ethyl)-amino]-phenyl} ester O-pentafluorophenyl ester

Guidance literature:: With triethylamine; In chloroform; at -10 ℃; for 1h;
DOI:10.1021/jm950671l

Reference yield:

: 101582-69-8
4--O-benzylphenol

: 174579-29-4
Thiocarbonic acid O-{4-[bis-(2-chloro-ethyl)-amino]-phenyl} ester O-pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 59 percent / CH₃SO₂Cl / pyridine / 0.83 h / 2 - 80 °C

2.1: HCl gas / methanol

2.2: 51 percent / H₂ / Pd/C / ethanol

3.1: Et₃N / toluene / 2 h / Heating

With hydrogenchloride; methanesulfonyl chloride; triethylamine; In pyridine; methanol; toluene;
DOI:10.1016/S0968-0896(01)00039-6

Reference yield:

: 17794-35-3
benzyl-p-(bis-2-chloroethylamino)phenyl ester

: 174579-29-4
Thiocarbonic acid O-{4-[bis-(2-chloro-ethyl)-amino]-phenyl} ester O-pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: HCl gas / methanol

1.2: 51 percent / H₂ / Pd/C / ethanol

2.1: Et₃N / toluene / 2 h / Heating

With hydrogenchloride; triethylamine; In methanol; toluene;
DOI:10.1016/S0968-0896(01)00039-6