N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-3-methylphenyl]-2-iodobenzamide

Base Information

Chemical Name:N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-3-methylphenyl]-2-iodobenzamide
CAS No.:1307740-98-2
Molecular Formula:C₂₁H₂₀F₆INO₂
Molecular Weight:559.29
Hs Code.:

Synonyms:N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-3-methylphenyl]-2-iodobenzamide

Suppliers and Price of N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-3-methylphenyl]-2-iodobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-3-methylphenyl]-2-iodobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-3-methylphenyl]-2-iodobenzamide

There total 2 articles about N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-3-methylphenyl]-2-iodobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 609-67-6
2-Iodobenzoyl chloride

: 1307740-88-0
2-(4-butylamino-2-methylphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol

: 1307740-98-2
N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-3-methylphenyl]-2-iodobenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1016/j.bmc.2011.03.002

Reference yield:

: 60995-75-7
N-butyl-m-toluidine

: 1307740-98-2
N-butyl-N-[4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-3-methylphenyl]-2-iodobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 10 h / 120 °C

2: triethylamine / dichloromethane / 3 h / 0 °C

With toluene-4-sulfonic acid; triethylamine; In dichloromethane; toluene;
DOI:10.1016/j.bmc.2011.03.002