tert-butylaminotriphenylphosphonium bromide

Base Information

Chemical Name:tert-butylaminotriphenylphosphonium bromide
CAS No.:799-51-9
Molecular Formula:Br*C₂₂H₂₅NP
Molecular Weight:414.325
Hs Code.:

Synonyms:tert-butylaminotriphenylphosphonium bromide

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Chemical Property of tert-butylaminotriphenylphosphonium bromide

Chemical Property:

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Technology Process of tert-butylaminotriphenylphosphonium bromide

There total 3 articles about tert-butylaminotriphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75-64-9
tert-butylamine

: 603-35-0
triphenylphosphine

: 799-51-9
tert-butylaminotriphenylphosphonium bromide

Guidance literature:: triphenylphosphine; With bromine; In dichloromethane; at -78 ℃; for 0.5h; Inert atmosphere;

tert-butylamine; With triethylamine; In dichloromethane; Inert atmosphere;
DOI:10.1021/om300389v

Reference yield:

: 5758-24-7
bromotriphenylphosphonium bromide

: 75-64-9
tert-butylamine

: 799-51-9
tert-butylaminotriphenylphosphonium bromide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/b618401d

Reference yield:

: 603-35-0
triphenylphosphine

: 799-51-9
tert-butylaminotriphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / CH₂Cl₂ / -78 - 20 °C

2: 6.0 g / Et₃N / CH₂Cl₂ / 2 h / 20 °C

With bromine; triethylamine; In dichloromethane;
DOI:10.1039/b618401d