Ac-Tyr(PO₃H₂)-Glu-Thr-Leu-Gly-OH

Base Information

Chemical Name:Ac-Tyr(PO₃H₂)-Glu-Thr-Leu-Gly-OH
CAS No.:1030021-84-1
Molecular Formula:C₂₈H₄₂N₅O₁₄P
Molecular Weight:703.64
Hs Code.:

Ac-Tyr(PO<sub>3</sub>H<sub>2</sub>)-Glu-Thr-Leu-Gly-OH

Synonyms:Ac-Tyr(PO₃H₂)-Glu-Thr-Leu-Gly-OH

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Chemical Property of Ac-Tyr(PO₃H₂)-Glu-Thr-Leu-Gly-OH

Chemical Property:

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Technology Process of Ac-Tyr(PO₃H₂)-Glu-Thr-Leu-Gly-OH

There total 3 articles about Ac-Tyr(PO₃H₂)-Glu-Thr-Leu-Gly-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Fmoc-Gly-Wang resin

: 35661-60-0
Fmoc-Leu-OH

: 71989-18-9
Fmoc-Glu(OtBu)-OH

: 108-24-7
acetic anhydride

: 71989-35-0,138797-71-4
Fmoc-Thr(tBu)-OH

: 191348-16-0
(S)-3-[4-(Benzyloxy-hydroxy-phosphoryloxy)-phenyl]-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid

: 1030021-96-5
C₂₈H₄₂N₅O₁₄P

: 1030021-84-1
Ac-Tyr(PO₃H₂)-Glu-Thr-Leu-Gly-OH

Guidance literature:: Fmoc-Gly-Wang resin; With piperidine; In N,N-dimethyl-formamide; for 0.0333333h; Automated synthesizer; solid phase reaction;

Fmoc-Leu-OH; With 4-methyl-morpholine; 1-[bis(dimethylamino)methylene]-5-chloro-1H-benzotriazolium-3-oxide tetrafluoroborate; In N,N-dimethyl-formamide; Automated synthesizer; solid phase reaction;

Fmoc-Glu(OtBu)-OH; acetic anhydride; Fmoc-Thr(tBu)-OH; (S)-3-[4-(Benzyloxy-hydroxy-phosphoryloxy)-phenyl]-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid; Automated synthesizer; solid phase reaction;
DOI:10.1039/b718568e

Reference yield:

: Fmoc-Gly-Wang resin

: 35661-60-0
Fmoc-Leu-OH

: 71989-18-9
Fmoc-Glu(OtBu)-OH

: 108-24-7
acetic anhydride

: 71989-35-0,138797-71-4
Fmoc-Thr(tBu)-OH

: 127633-36-7,201335-92-4
Fmoc-Tyr(PO(OMe)2)-OH

: 1030021-96-5
C₂₈H₄₂N₅O₁₄P

: 1030021-84-1
Ac-Tyr(PO₃H₂)-Glu-Thr-Leu-Gly-OH

Guidance literature:: Fmoc-Gly-Wang resin; With piperidine; In N,N-dimethyl-formamide; for 0.0333333h; Automated synthesizer; solid phase reaction;

Fmoc-Leu-OH; With 4-methyl-morpholine; 1-[bis(dimethylamino)methylene]-5-chloro-1H-benzotriazolium-3-oxide tetrafluoroborate; In N,N-dimethyl-formamide; Automated synthesizer; solid phase reaction;

Fmoc-Glu(OtBu)-OH; acetic anhydride; Fmoc-Thr(tBu)-OH; Fmoc-Tyr(PO(OMe)2)-OH; Automated synthesizer; solid phase reaction;
DOI:10.1039/b718568e

Reference yield:

: Fmoc-Gly-Wang resin

: 35661-60-0
Fmoc-Leu-OH

: 71989-18-9
Fmoc-Glu(OtBu)-OH

: 108-24-7
acetic anhydride

: 71989-35-0,138797-71-4
Fmoc-Thr(tBu)-OH

: 172611-23-3
(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4(bis(dimethylamino)phosphoryloxy)phenyl)propanoic acid

: 1030021-96-5
C₂₈H₄₂N₅O₁₄P

: 1030021-84-1
Ac-Tyr(PO₃H₂)-Glu-Thr-Leu-Gly-OH

Guidance literature:: Fmoc-Gly-Wang resin; With piperidine; In N,N-dimethyl-formamide; for 0.0333333h; Automated synthesizer; solid phase reaction;

Fmoc-Leu-OH; With 4-methyl-morpholine; 1-[bis(dimethylamino)methylene]-5-chloro-1H-benzotriazolium-3-oxide tetrafluoroborate; In N,N-dimethyl-formamide; Automated synthesizer; solid phase reaction;

Fmoc-Glu(OtBu)-OH; acetic anhydride; Fmoc-Thr(tBu)-OH; (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4(bis(dimethylamino)phosphoryloxy)phenyl)propanoic acid; Automated synthesizer; solid phase reaction;
DOI:10.1039/b718568e