Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)⁽¹⁺⁾*BF₄^(1-)=[Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)]BF₄

Base Information

• Chemical Name: Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)⁽¹⁺⁾*BF₄^(1-)=[Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)]BF₄
• CAS No.: 194282-26-3
• Molecular Formula: BF₄*C₃₃H₃₀NNiP₂S₂
• Molecular Weight: 712.182

Synonyms:Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)⁽¹⁺⁾*BF₄^(1-)=[Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)]BF₄

Chemical Property of Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)⁽¹⁺⁾*BF₄^(1-)=[Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)]BF₄

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Technology Process of Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)⁽¹⁺⁾*BF₄^(1-)=[Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)]BF₄

There total 2 articles about Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)⁽¹⁺⁾*BF₄^(1-)=[Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄NH)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Bromoacetylpyridine (40086-66-6) + (1,2-bis(diphenylphosphino)ethane)Ni(SH)2 (69679-64-7) → Ni((C6H5)2PCH2CH2P(C6H5)2)(S2C2HC5H4NH)(1+)*BF4(1-)=[Ni((C6H5)2PCH2CH2P(C6H5)2)(S2C2HC5H4NH)]BF4 (194282-26-3)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / N,N-dimethyl-formamide

2: dichloromethane

With Et₃N; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ic970194s

Reference yield:

tetrafluoroboric acid diethyl ether (67969-82-8) + Ni((C6H5)2PCH2CH2P(C6H5)2)(S2C2HC5H4N) (194282-25-2) → Ni((C6H5)2PCH2CH2P(C6H5)2)(S2C2HC5H4NH)(1+)*BF4(1-)=[Ni((C6H5)2PCH2CH2P(C6H5)2)(S2C2HC5H4NH)]BF4 (194282-26-3)

Guidance literature:

In dichloromethane; N2-atmosphere; dropwise addn. of HBF4 to metal complex (UV/VIS monitoring); in air; solvent removal, washing (Et2O);

DOI:10.1021/ic970194s

upstream raw materials:

tetrafluoroboric acid diethyl ether

Ni((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(S₂C₂HC₅H₄N)

2-Bromoacetylpyridine

(1,2-bis(diphenylphosphino)ethane)Ni(SH)2

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