C₅₀H₆₀O₁₀Si

Base Information

Chemical Name:C₅₀H₆₀O₁₀Si
CAS No.:1361049-76-4
Molecular Formula:C₅₀H₆₀O₁₀Si
Molecular Weight:849.106
Hs Code.:

C<sub>50</sub>H<sub>60</sub>O<sub>10</sub>Si

Synonyms:C₅₀H₆₀O₁₀Si

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Chemical Property of C₅₀H₆₀O₁₀Si

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Technology Process of C₅₀H₆₀O₁₀Si

There total 16 articles about C₅₀H₆₀O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1361049-66-2
C₄₃H₅₆O₉Si

: 98-88-4
benzoyl chloride

: 1361049-76-4
C₅₀H₆₀O₁₀Si

Guidance literature:: With dmap; triethylamine; at 20 ℃; for 18h;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-71-9
C₁₆H₂₆O₆Si

: 1361049-76-4
C₅₀H₆₀O₁₀Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

1.2: 21 h / 20 °C

2.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

3.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

3.2: 0.5 h / 0 °C

4.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

5.1: acetone; acetonitrile / 2 h / Irradiation

5.2: 16 h / 20 °C / 760.05 Torr

6.1: t-butyldimethylsiyl triflate / hexane; dichloromethane / 12 h / 0 °C / Molecular sieve

7.1: tetrahydrofuran; diethyl ether / -78 °C

8.1: methanol; potassium carbonate / tetrahydrofuran

9.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C

10.1: dmap; triethylamine / 18 h / 20 °C

With 4-methyl-morpholine; methanol; dmap; barium hydroxide octahydrate; t-butyldimethylsiyl triflate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; triethylamine; methyl chloroformate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-61-7
C₂₂H₃₀O₆Si

: 1361049-76-4
C₅₀H₆₀O₁₀Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

1.2: 0.5 h / 0 °C

2.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

3.1: acetone; acetonitrile / 2 h / Irradiation

3.2: 16 h / 20 °C / 760.05 Torr

4.1: t-butyldimethylsiyl triflate / hexane; dichloromethane / 12 h / 0 °C / Molecular sieve

5.1: tetrahydrofuran; diethyl ether / -78 °C

6.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C

7.1: dmap; triethylamine / 18 h / 20 °C

With 4-methyl-morpholine; dmap; t-butyldimethylsiyl triflate; pyridinium p-toluenesulfonate; triethylamine; methyl chloroformate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; acetone; acetonitrile;
DOI:10.1002/anie.201106889