Technology Process of C30H28N2O5S2
There total 4 articles about C30H28N2O5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(1S,2S)-N-(4-cyanophenyl)-1-(4-methoxyphenyl)-2-(methylsulfenyl)-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine;
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
With
sodium hydrogencarbonate;
In
dichloromethane;
Inert atmosphere;
DOI:10.1021/ol201696y
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene / 24 h / Molecular sieve; Reflux; Inert atmosphere
2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.02 h / -78 °C / Inert atmosphere
2.2: 0.02 h / -78 °C / Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere
3.2: Inert atmosphere
With
n-butyllithium; diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/ol201696y
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene / 24 h / Molecular sieve; Reflux; Inert atmosphere
2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.02 h / -78 °C / Inert atmosphere
2.2: 0.02 h / -78 °C / Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere
3.2: Inert atmosphere
With
n-butyllithium; diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/ol201696y
![(1S,2S)-N-(4-cyanophenyl)-1-(4-methoxyphenyl)-2-(methylsulfenyl)-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine](/Databaselist/images/loading.webp)
