2-(1-METHYL-4-OXO-1,4-DIHYDRO-QUINOLIN-3-YL)-BENZOIC ACID METHYL ESTER

Base Information

• Chemical Name: 2-(1-METHYL-4-OXO-1,4-DIHYDRO-QUINOLIN-3-YL)-BENZOIC ACID METHYL ESTER
• CAS No.: 294184-16-0
• Molecular Formula: C₁₈H₁₅NO₃
• Molecular Weight: 293.322
• Hs Code.: 2933499090
• Mol file: 294184-16-0.mol

Synonyms:3-(2-Methoxycarbonylphenyl)-1-methyl-4-oxo-1,4-dihydroquinoline

Chemical Property of 2-(1-METHYL-4-OXO-1,4-DIHYDRO-QUINOLIN-3-YL)-BENZOIC ACID METHYL ESTER

Chemical Property:

Purity/Quality:

METHYL 2-(1-METHYL-4-OXO-1,4-DIHYDRO-3-QUINOLINYL)BENZENECARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

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Technology Process of 2-(1-METHYL-4-OXO-1,4-DIHYDRO-QUINOLIN-3-YL)-BENZOIC ACID METHYL ESTER

There total 1 articles about 2-(1-METHYL-4-OXO-1,4-DIHYDRO-QUINOLIN-3-YL)-BENZOIC ACID METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

methanol (67-56-1) + 12-Methyl-6-oxo-6H-<2>benzopyrano<4,3-c>quinolinium phosphorodichloridate → 3-(2-Methoxycarbonylphenyl)-1-methyl-4-oxo-1,4-dihydroquinoline (294184-16-0)

Guidance literature:

With sulfuric acid; for 3h; Heating;

DOI:10.1055/s-2000-6325

Reference yield: 55.0%

3-(2-Methoxycarbonylphenyl)-1-methyl-4-oxo-1,4-dihydroquinoline (294184-16-0) → 3-(2-Hydroxymethylphenyl)-1-methyl-4-oxo-1,4-dihydroquinoline

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1055/s-2000-6325

Reference yield:

3-(2-Methoxycarbonylphenyl)-1-methyl-4-oxo-1,4-dihydroquinoline (294184-16-0) → 6-Dihydro-12-methyl-[2]benzopyrano[4,3-c]quinolinium p-toluenesulfonate

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / LiAlH₄ / tetrahydrofuran / 12 h / 20 °C

2: 76 percent / toluene / 1.5 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; toluene; 1: Reduction / 2: Cyclization;

DOI:10.1055/s-2000-6325

upstream raw materials:

methanol

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