C₃₀H₂₈F₂N₆O₂

Base Information

Chemical Name:C₃₀H₂₈F₂N₆O₂
CAS No.:1345438-96-1
Molecular Formula:C₃₀H₂₈F₂N₆O₂
Molecular Weight:542.588
Hs Code.:

C<sub>30</sub>H<sub>28</sub>F<sub>2</sub>N<sub>6</sub>O<sub>2</sub>

Synonyms:C₃₀H₂₈F₂N₆O₂

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Chemical Property of C₃₀H₂₈F₂N₆O₂

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Technology Process of C₃₀H₂₈F₂N₆O₂

There total 10 articles about C₃₀H₂₈F₂N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1345438-94-9
C₂₉H₂₆F₂N₆O₂

: 1345438-96-1
C₃₀H₂₈F₂N₆O₂

Guidance literature:: formaldehyd; C₂₉H₂₆F₂N₆O₂; With acetic acid; In ISOPROPYLAMIDE; at 20 ℃; for 1h;

With sodium tris(acetoxy)borohydride; In ISOPROPYLAMIDE; at 20 ℃; for 12h;

Reference yield:

: 85118-01-0
alpha-bromo-3,4-difluorotoluene

: 1345438-96-1
C₃₀H₂₈F₂N₆O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 20 °C

1.2: 3 h / 20 °C

2.1: sodium hydroxide / methanol / 16 h / 20 °C

2.2: Acidic conditions

3.1: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 12 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; copper(l) iodide / [Pd⁰(1,1’-bis(diphenylphosphino)ferrocene)] / dimethyl sulfoxide / 3 h / 50 °C

5.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

6.1: acetic acid / ISOPROPYLAMIDE / 1 h / 20 °C

6.2: 12 h / 20 °C

With copper(l) iodide; sodium hydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; [Pd⁰(1,1’-bis(diphenylphosphino)ferrocene)]; In methanol; dichloromethane; ISOPROPYLAMIDE; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 89891-65-6
7-bromo-2-chloroquinoxaline

: 1345438-96-1
C₃₀H₂₈F₂N₆O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / N,N-dimethyl-formamide / 1 h / 65 °C

1.2: 20 - 60 °C

2.1: N-ethyl-N,N-diisopropylamine; copper(l) iodide / [Pd⁰(1,1’-bis(diphenylphosphino)ferrocene)] / dimethyl sulfoxide / 3 h / 50 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4.1: acetic acid / ISOPROPYLAMIDE / 1 h / 20 °C

4.2: 12 h / 20 °C

With copper(l) iodide; acetic acid; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; trifluoroacetic acid; [Pd⁰(1,1’-bis(diphenylphosphino)ferrocene)]; In dichloromethane; ISOPROPYLAMIDE; dimethyl sulfoxide; N,N-dimethyl-formamide;