methyl 2-cyano-3-{4-[(3-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Base Information

Chemical Name:methyl 2-cyano-3-{4-[(3-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate
CAS No.:1356599-93-3
Molecular Formula:C₂₇H₂₆N₂O₅
Molecular Weight:458.514
Hs Code.:

Synonyms:methyl 2-cyano-3-{4-[(3-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

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Chemical Property of methyl 2-cyano-3-{4-[(3-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

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Technology Process of methyl 2-cyano-3-{4-[(3-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

There total 7 articles about methyl 2-cyano-3-{4-[(3-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.85%

: 1356599-92-2
methyl 2-cyano-3-{4-[(3-hydroxybenzyl)oxy]phenyl}propanoate

: 142533-52-6
(Z)-2-bromo-1-phenylethanone O-methyl oxime

: 1356599-93-3
methyl 2-cyano-3-{4-[(3-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: With potassium carbonate; In acetonitrile; at 50 ℃; for 1h;

Reference yield:

: 28166-41-8
α-cyano-4-hydroxycinnamic acid

: 1356599-93-3
methyl 2-cyano-3-{4-[(3-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 72 h / 20 °C / 1551.49 Torr

2: methanesulfonic acid / 1 h / 65 °C

3: potassium carbonate / acetonitrile / 1 h / 50 °C

4: potassium carbonate / acetonitrile / 1 h / 50 °C

With methanesulfonic acid; hydrogen; potassium carbonate; palladium 10% on activated carbon; In ethyl acetate; acetonitrile;

Reference yield:

: 620-24-6
3-Hydroxybenzyl alcohol

: 1356599-93-3
methyl 2-cyano-3-{4-[(3-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide / dichloromethane / 1 h / 0 - 20 °C

2: potassium carbonate / acetonitrile / 1 h / 50 °C

3: potassium carbonate / acetonitrile / 1 h / 50 °C

With phosphorus tribromide; potassium carbonate; In dichloromethane; acetonitrile;