Mo(C₅H₅)(S₂C₂(C₆H₅)2)2

Base Information

Chemical Name:Mo(C₅H₅)(S₂C₂(C₆H₅)2)2
CAS No.:923001-21-2
Molecular Formula:C₃₃H₂₅MoS₄
Molecular Weight:645.766
Hs Code.:

Mo(C<sub>5</sub>H<sub>5</sub>)(S<sub>2</sub>C<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2)2

Synonyms:Mo(C₅H₅)(S₂C₂(C₆H₅)2)2

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Chemical Property of Mo(C₅H₅)(S₂C₂(C₆H₅)2)2

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Technology Process of Mo(C₅H₅)(S₂C₂(C₆H₅)2)2

There total 2 articles about Mo(C₅H₅)(S₂C₂(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: Ni(Mo(C₅H₅)(S₂C₂(C₆H₅)2)2)2

: 923001-21-2
Mo(C₅H₅)(S₂C₂(C₆H₅)2)2

Guidance literature:: With sulfur; In toluene; (under Ar or N2); soln. of NiMo-complex and S in toluene refluxed for 2.5 h; solvent removed, column chromy. on silica with hexane-CH2Cl2;
DOI:10.1021/ic0606227

Reference yield: 19.8%

: 12128-23-3
tricarbonylcyclopentadienylmolybdenum(II) chloride

: 28984-20-5
bis(1,2-diphenylethylene-1,2-ditholate) nickel(IV)

: 923001-21-2
Mo(C₅H₅)(S₂C₂(C₆H₅)2)2

: Ni(Mo(C₅H₅)(S₂C₂(C₆H₅)2)2)2*4C₄H₈O

Guidance literature:: In toluene; (under Ar or N2); Mo- and Ni-complexes dissolved in toluene, refluxed for 2 h; solvent removed in vac., residue redissolved in CH2Cl2, silica column chromy. with light petroleum or hexane, eluted with hexane-CH2Cl2 4:1, 13:7, 2:3 for 1.5 h; elem. anal.;
DOI:10.1021/ic0606227

Reference yield: 85.0%

: 1271-28-9
nickelocene

: 923001-21-2
Mo(C₅H₅)(S₂C₂(C₆H₅)2)2

: NiMo(μ-S2C2Ph2)2Cp2

Guidance literature:: In toluene; (under Ar or N2); Mo- and Ni-complexes dissolved in toluene, refluxed for 1 h; silica column chromy. with petroleum ether or hexane, eluted with hexane-CH2Cl2; elem. anal.;
DOI:10.1021/ic0606227