2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine

Base Information

Chemical Name:2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine
CAS No.:870196-21-7
Molecular Formula:C₃₆H₄₇NOSSi₂
Molecular Weight:598.012
Hs Code.:

2-(<i>tert</i>-butyl-diphenyl-silanyloxy)-1-(<i>tert</i>-butyl-diphenyl-silanylsulfanylmethyl)-propylamine

Synonyms:2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine

Suppliers and Price of 2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine

There total 7 articles about 2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 870196-20-6
[2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propyl]-carbamic acid tert-butyl ester

: 870196-21-7
2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 23 ℃; for 0.333333h;
DOI:10.1016/j.bmcl.2005.07.073

Reference yield:

: 870196-19-3
[1-bromomethyl-2-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid tert-butyl ester

: 870196-21-7
2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / tetrahydrofuran / 19 h / -78 - 23 °C

2: 82 percent / HCl / ethyl acetate / 0.33 h / 23 °C

With hydrogenchloride; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.bmcl.2005.07.073

Reference yield:

: 870196-18-2
[2-(tert-butyl-diphenyl-silanyloxy)-1-hydroxymethyl-propyl]-carbamic acid tert-butyl ester

: 870196-21-7
2-(tert-butyl-diphenyl-silanyloxy)-1-(tert-butyl-diphenyl-silanylsulfanylmethyl)-propylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / Et₃N; PPh₃; CBr₄ / CH₂Cl₂ / 18 h / 23 °C

2: 96 percent / tetrahydrofuran / 19 h / -78 - 23 °C

3: 82 percent / HCl / ethyl acetate / 0.33 h / 23 °C

With hydrogenchloride; carbon tetrabromide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2005.07.073