methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate

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Chemical Name:methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate
CAS No.:553679-29-1
Molecular Formula:C₃₈H₄₀F₃NO₁₂S
Molecular Weight:791.796
Hs Code.:

methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate

Synonyms:methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate

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Chemical Property of methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate

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Technology Process of methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate

There total 12 articles about methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 553679-28-0
dimethyl 2-[2-(3-{(1R)-2-[(4-methylphenyl)sulfonyloxy]-1-phenylcarbonyloxyethyl}(2R,3R)oxiran-2-yl)prop-2-enyl]-4-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}(2S,4S)-2-hydroxypentane-1,5-dioate

: 553679-29-1
methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate

Guidance literature:: In chloroform; at 20 ℃; for 12h;

Reference yield: 4.4%

: 553679-28-0
dimethyl 2-[2-(3-{(1R)-2-[(4-methylphenyl)sulfonyloxy]-1-phenylcarbonyloxyethyl}(2R,3R)oxiran-2-yl)prop-2-enyl]-4-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}(2S,4S)-2-hydroxypentane-1,5-dioate

: (1R)-1-{3-[1-({4-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}(4S,2R)-2-(methocycarbonyl)-5-oxo(2-2,3,4-trihydrofuryl)}methyl)vinyl](2R,3R)oxiran-2-yl}-3-[(4-methylphenyl)sulfonyl]propylbenzoate

: 553679-29-1
methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 98-88-4
benzoyl chloride

: 553679-29-1
methyl 2-{N-[(1R)-1-phenylethyl]-2,2,2-trifluoroacetylamino}-3-(5-{(1R,2R)-1-hydroxy-3-[(4-methylphenyl)sulfonyloxy]-2-phenylcarbonyloxypropyl}(2S)-2-(methoxycarbonyl)-4-methylene(2-2,3,5-trihydrofuryl))(2S)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine / 2 h / 0 °C

2: 85 percent / CSA / CH₂Cl₂ / 16 h / 20 °C

With pyridine; camphor-10-sulfonic acid; In dichloromethane;