3-(2-hydroxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one

Base Information

• Chemical Name: 3-(2-hydroxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one
• CAS No.: 221203-07-2
• Molecular Formula: C₂₀H₂₀N₂O₂
• Molecular Weight: 320.391

Synonyms:3-(2-hydroxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one

Chemical Property of 3-(2-hydroxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one

Chemical Property:

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Technology Process of 3-(2-hydroxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one

There total 1 articles about 3-(2-hydroxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

tetrahydrobetacarboline (16502-01-5) + C6H4(CH2CH2C(O)O) (119-84-6,1341-36-2) → 3-(2-hydroxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one (221203-07-2)

Guidance literature:

With water; In tetrahydrofuran;

DOI:10.1016/S0040-4039(98)02598-2

Reference yield:

3-(2-hydroxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one (221203-07-2) → 2-[3-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propyl]-phenol

Guidance literature:

With methanol; AG 50W-X₂₁₀; diborane; In tetrahydrofuran; Yield given; 1.) 50 deg C; 2.) r.t.;

DOI:10.1016/S0040-4039(98)02598-2

Reference yield:

methanol (67-56-1) + 3-(2-hydroxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one (221203-07-2) → 3-(2-methoxy-phenyl)-1-(1,3,4,9-tetrahydro-β-carbolin-2-yl)-propan-1-one

Guidance literature:

With WA₂IJ resin; In tetrahydrofuran; Yield given;

DOI:10.1016/S0040-4039(98)02598-2

upstream raw materials:

tetrahydrobetacarboline

C₆H₄(CH₂CH₂C(O)O)

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