p-nitrobenzyl acetohydroxamate

Base Information

• Chemical Name: p-nitrobenzyl acetohydroxamate
• CAS No.: 100704-42-5
• Molecular Formula: C₉H₁₀N₂O₄
• Molecular Weight: 210.189
• Mol file: 100704-42-5.mol

Synonyms:p-nitrobenzyl acetohydroxamate

Chemical Property of p-nitrobenzyl acetohydroxamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of p-nitrobenzyl acetohydroxamate

There total 2 articles about p-nitrobenzyl acetohydroxamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

potassium acetoxyhydroxamate (23654-87-7) + 1-bromomethyl-4-nitro-benzene (100-11-8) → p-nitrobenzyl acetohydroxamate (100704-42-5)

Guidance literature:

With sodium carbonate; In methanol; water; 1) room temperature, 24 h, 2) reflux, 2 h;

DOI:10.1016/S0040-4020(98)01151-X

Reference yield:

4-nitrobenzyl chloride (100-14-1) + ethyl acetate (141-78-6) → p-nitrobenzyl acetohydroxamate (100704-42-5)

Guidance literature:

Multistep reaction; (i) NaOMe, NH₂OH*HCl, MeOH, (ii) /BRN= 387187/, aq. Na₂CO₃;

DOI:10.1021/jo01080a014

Reference yield:

p-nitrobenzyl acetohydroxamate (100704-42-5) → N,N'-diacetyl-N,N'-di-(p-nitrobenzyloxy)hydrazine (62250-55-9)

Guidance literature:

With lead(IV) acetate; In benzene;

DOI:10.1021/ja01009a032

upstream raw materials:

4-nitrobenzyl chloride

ethyl acetate

potassium acetoxyhydroxamate

1-bromomethyl-4-nitro-benzene

Downstream raw materials:

N,N'-diacetyl-N,N'-di-(p-nitrobenzyloxy)hydrazine

N-Nitroso-N-acetyl-O-(4-nitro-benzyl)-hydroxylamin