Technology Process of C11H16NO6P
There total 3 articles about C11H16NO6P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; ammonium formate;
In
methanol;
for 0.333333h;
Reflux;
DOI:10.1021/jm301577q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C
1.2: 0.25 h / -78 °C
2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 30 °C / Sonication
3.1: ammonium formate; palladium 10% on activated carbon / methanol / 0.33 h / Reflux
With
di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium formate; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol;
DOI:10.1021/jm301577q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium osmate(VI) dihydrate; sodium periodate / tetrahydrofuran; water / 4 h / Darkness
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C
2.2: 0.25 h / -78 °C
3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 30 °C / Sonication
4.1: ammonium formate; palladium 10% on activated carbon / methanol / 0.33 h / Reflux
With
potassium osmate(VI) dihydrate; sodium periodate; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium formate; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; water;
DOI:10.1021/jm301577q
