1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole

Base Information

Chemical Name:1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole
CAS No.:1146972-70-4
Molecular Formula:C₁₉H₂₀N₂O₅S
Molecular Weight:388.444
Hs Code.:

Synonyms:1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole

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Chemical Property of 1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole

Chemical Property:

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Technology Process of 1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole

There total 2 articles about 1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21987-25-7
5-methoxy-3-methyl-1H-indole

: 3746-67-6
3-(acetylamino)-4-methoxybenzensulfonyl chloride

: 1146972-70-4
1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole

Guidance literature:: 5-methoxy-3-methyl-1H-indole; With sodium hydride; In tetrahydrofuran; at 25 ℃; for 1.25h;

3-(acetylamino)-4-methoxybenzensulfonyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 24.3333h;

Reference yield:

: 93-26-5
2-methoxyacetanilide

: 1146972-70-4
1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: chlorosulfonic acid / 26 h / 20 - 100 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere

2.2: 24 h / 0 - 20 °C / Inert atmosphere

With chlorosulfonic acid; sodium hydride; In tetrahydrofuran;
DOI:10.3109/14756366.2014.889126

Reference yield:

: 1146972-70-4
1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole

: 1146972-71-5
1-(3'-amino-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole

Guidance literature:: 1-(3'-acetamido-4'-methoxybenzenesulfonyl)-5-methoxy-3-methyl-1H-indole; With hydrogenchloride; water; In ethanol; for 2h; Heating / reflux;

With sodium hydroxide; In water; pH=9 - 10;