(Z)-2-[(4-aminophenyl)-(4-methylsemicarbazono)-methyl]-4,5-methylenedioxyphenylacetic acid methyl ester

Base Information

Chemical Name:(Z)-2-[(4-aminophenyl)-(4-methylsemicarbazono)-methyl]-4,5-methylenedioxyphenylacetic acid methyl ester
CAS No.:473451-42-2
Molecular Formula:C₁₉H₂₀N₄O₅
Molecular Weight:384.392
Hs Code.:

Synonyms:(Z)-2-[(4-aminophenyl)-(4-methylsemicarbazono)-methyl]-4,5-methylenedioxyphenylacetic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-[(4-aminophenyl)-(4-methylsemicarbazono)-methyl]-4,5-methylenedioxyphenylacetic acid methyl ester

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Technology Process of (Z)-2-[(4-aminophenyl)-(4-methylsemicarbazono)-methyl]-4,5-methylenedioxyphenylacetic acid methyl ester

There total 2 articles about (Z)-2-[(4-aminophenyl)-(4-methylsemicarbazono)-methyl]-4,5-methylenedioxyphenylacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 67-56-1
methanol

: 221903-94-2
3,5-dihydro-3-N-methylcarbamoyl-7,8-methylenedioxy-1-(4-nitrophenyl)-4H-2,3-benzodiazepin-4-one

: 473451-42-2
(Z)-2-[(4-aminophenyl)-(4-methylsemicarbazono)-methyl]-4,5-methylenedioxyphenylacetic acid methyl ester

Guidance literature:: With tin(ll) chloride; at 80 ℃; for 2h;
DOI:10.1021/jm020863y

Reference yield:

: 194729-10-7
7,8-methylenedioxy-1-(4-nitrophenyl)-3,5-dihydro-2,3-benzodiazepin-4(4H)-one

: 473451-42-2
(Z)-2-[(4-aminophenyl)-(4-methylsemicarbazono)-methyl]-4,5-methylenedioxyphenylacetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / triethylamine / CH₂Cl₂ / 36 h / 20 °C

2: 82 percent / tin(II) chloride / 2 h / 80 °C

With triethylamine; tin(ll) chloride; In dichloromethane;
DOI:10.1021/jm020863y