methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

Base Information

Chemical Name:methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside
CAS No.:142466-95-3
Molecular Formula:C₇₁H₈₁NO₁₅
Molecular Weight:1188.42
Hs Code.:

methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

Synonyms:methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

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Chemical Property of methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

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Technology Process of methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

There total 9 articles about methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 142466-94-2
methyl 2-acetamido-3-O-benzyl-2-deoxy-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

: 74-88-4
methyl iodide

: 142466-95-3
methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

Guidance literature:: With barium dihydroxide; barium(II) oxide; In N,N-dimethyl-formamide; for 20h; Ambient temperature;

Reference yield:

: 69892-45-1
methyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

: 142466-95-3
methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: 77 percent / pyridine / 1.17 h / -20 °C

2: 74 percent / Hg(CN)2 / toluene; nitromethane / 1 h / 40 °C

3: 75 percent / sodium methoxide / methanol

4: 90 percent / Et₄NBr, 4 Angstroem molecular sieves / CH₂Cl₂; dimethylformamide / 20 h / Ambient temperature

5: 84 percent / dimethylformamide / 4.5 h / 100 °C

6: 98 percent / sodium methoxide / methanol / 20 h / Ambient temperature

7: 79 percent / BaO, Ba(OH)2*8H₂O / dimethylformamide / 20 h / Ambient temperature

With pyridine; barium dihydroxide; 4 A molecular sieve; tetraethylammonium bromide; sodium methylate; mercury(II) cyanide; barium(II) oxide; In methanol; nitromethane; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 100-39-0
benzyl bromide

: 142466-95-3
methyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-methyl-4-O-<3,4,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranosyl>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 9 steps

1: 82 percent / BaO, Ba(OH)2*8H₂O / dimethylformamide / 2 h

2: 96 percent / 80percent acetic acid / 0.25 h / 80 °C

3: 77 percent / pyridine / 1.17 h / -20 °C

4: 74 percent / Hg(CN)2 / toluene; nitromethane / 1 h / 40 °C

5: 75 percent / sodium methoxide / methanol

6: 90 percent / Et₄NBr, 4 Angstroem molecular sieves / CH₂Cl₂; dimethylformamide / 20 h / Ambient temperature

7: 84 percent / dimethylformamide / 4.5 h / 100 °C

8: 98 percent / sodium methoxide / methanol / 20 h / Ambient temperature

9: 79 percent / BaO, Ba(OH)2*8H₂O / dimethylformamide / 20 h / Ambient temperature

With pyridine; barium dihydroxide; 4 A molecular sieve; tetraethylammonium bromide; sodium methylate; mercury(II) cyanide; acetic acid; barium(II) oxide; In methanol; nitromethane; dichloromethane; N,N-dimethyl-formamide; toluene;