bis(2-methylphenyl)iodonium hexafluorophosphate

Base Information

• Chemical Name: bis(2-methylphenyl)iodonium hexafluorophosphate
• CAS No.: 91290-91-4
• Molecular Formula: C₁₄H₁₄I*F₆P
• Molecular Weight: 454.134
• Mol file: 91290-91-4.mol

Synonyms:bis(2-methylphenyl)iodonium hexafluorophosphate

Chemical Property of bis(2-methylphenyl)iodonium hexafluorophosphate

Chemical Property:

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Technology Process of bis(2-methylphenyl)iodonium hexafluorophosphate

There total 1 articles about bis(2-methylphenyl)iodonium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid (1374643-16-9) → bis(2-methylphenyl)iodonium hexafluorophosphate (91290-91-4)

Guidance literature:

With potassium hexafluorophosphate; In acetonitrile; for 24h; Inert atmosphere; Sealed tube;

DOI:10.1021/ol501655g

Reference yield: 82.0%

bis(2-methylphenyl)iodonium hexafluorophosphate (91290-91-4) + anthranilic acid nitrile (1885-29-6) → 2-(3-(2-methylphenyl)-4-imino-3,4-dihydroquinazoline)-2-aniline

Guidance literature:

In 1,2-dichloro-ethane; at 20 - 120 ℃; for 48h; Inert atmosphere;

Reference yield: 81.0%

bis(2-methylphenyl)iodonium hexafluorophosphate (91290-91-4) + 4-(2-isothiocyanatoethyl)-1,2-dimethoxybenzene (21714-25-0) → 6,7-dimethoxy-1-(o-tolylthio)-3,4-dihydroisoquinoline

Guidance literature:

With copper(l) chloride; In 1,2-dichloro-ethane; at 80 ℃; for 2h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.joc.6b02605

upstream raw materials:

bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid