3-(2-methoxyphenyl)propynoic acid benzylchrysen-6-ylamide

Base Information

Chemical Name:3-(2-methoxyphenyl)propynoic acid benzylchrysen-6-ylamide
CAS No.:1394233-09-0
Molecular Formula:C₃₅H₂₅NO₂
Molecular Weight:491.589
Hs Code.:

Synonyms:3-(2-methoxyphenyl)propynoic acid benzylchrysen-6-ylamide

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Chemical Property of 3-(2-methoxyphenyl)propynoic acid benzylchrysen-6-ylamide

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Technology Process of 3-(2-methoxyphenyl)propynoic acid benzylchrysen-6-ylamide

There total 3 articles about 3-(2-methoxyphenyl)propynoic acid benzylchrysen-6-ylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394233-28-3
C₂₈H₁₉NO₂

: 100-39-0
benzyl bromide

: 1394233-09-0
3-(2-methoxyphenyl)propynoic acid benzylchrysen-6-ylamide

Guidance literature:: C₂₈H₁₉NO₂; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at 0 - 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1002/anie.201202165

Reference yield:

: 2642-98-0
6-aminochrysene

: 1394233-09-0
3-(2-methoxyphenyl)propynoic acid benzylchrysen-6-ylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: HATU / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 h / 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 3.5 h / 0 - 20 °C / Inert atmosphere

With sodium hydride; HATU; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.201202165

Reference yield:

: 7342-00-9
3-(2-methoxyphenyl)prop-2-ynoic acid

: 1394233-09-0
3-(2-methoxyphenyl)propynoic acid benzylchrysen-6-ylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: HATU / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 h / 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 3.5 h / 0 - 20 °C / Inert atmosphere

With sodium hydride; HATU; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.201202165